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@ARTICLE{Dargatz:280718,
      author       = {Dargatz, Benjamin and Gonzalez, Jesus and Bram, Martin and
                      Jakes, Peter and Besmehn, Astrid and Schade, Lisa and
                      Röder, Robert and Ronning, Carsten and Guillon, Olivier},
      title        = {{FAST}/{SPS} sintering of nanocrystalline zinc
                      oxide—{P}art {I}: {E}nhanced densification and formation
                      of hydrogen-related defects in presence of adsorbed water},
      journal      = {Journal of the European Ceramic Society},
      volume       = {36},
      number       = {5},
      issn         = {0955-2219},
      address      = {Amsterdam [u.a.]},
      publisher    = {Elsevier Science},
      reportid     = {FZJ-2016-00475},
      pages        = {1207-1220},
      year         = {2016},
      abstract     = {This part is focused on the effect of surface bound water
                      on the densification behavior and defect stoichiometry of
                      zinc oxide. The second part [doi:
                      10.1016/j.jeurceramsoc.2015.12.008] concentrates on the
                      effect of hydroxide complexions on the microstructural
                      development, texture formation and anisotropic grain
                      morphology. Nanocrystalline zinc oxide powder was humidified
                      or dried followed by quick heating (100 K/min) with
                      field-assisted sintering technique/spark plasma sintering
                      (FAST/SPS). Densification is strongly enhanced due to
                      hydroxide-ion-diffusion mechanism, which shows species with
                      lower valence and ionic radius in comparison to oxygen ions.
                      The lowered activation energy for densification exhibits no
                      impact of the sintering electric current on this enhanced
                      densification behavior. The defect stoichiometry and
                      structure of sintered zinc oxide was analyzed by several
                      spectroscopic methods, indicating the formation of
                      hydrogen-related defects for sintering in presence of bound
                      water, while no hydrogen was detected for sintering of dried
                      powder.},
      cin          = {IEK-1 / JARA-ENERGY / IEK-9 / ZEA-3},
      ddc          = {660},
      cid          = {I:(DE-Juel1)IEK-1-20101013 / $I:(DE-82)080011_20140620$ /
                      I:(DE-Juel1)IEK-9-20110218 / I:(DE-Juel1)ZEA-3-20090406},
      pnm          = {899 - ohne Topic (POF3-899)},
      pid          = {G:(DE-HGF)POF3-899},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000369457300011},
      doi          = {10.1016/j.jeurceramsoc.2015.12.009},
      url          = {https://juser.fz-juelich.de/record/280718},
}