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@ARTICLE{BellissentFunel:281859,
author = {Bellissent-Funel, Marie-Claire and Kaneko, Katsumi and
Ohba, Tomonori and Appavou, Marie-Sousai and Soininen, Antti
and Wuttke, Joachim},
title = {{C}rossover from localized to diffusive water dynamics in
carbon nanohorns: {A} comprehensive quasielastic
neutron-scattering analysis},
journal = {Physical review / E},
volume = {93},
number = {2},
issn = {2470-0045},
address = {College Park, Md.},
publisher = {APS},
reportid = {FZJ-2016-01521},
pages = {022104},
year = {2016},
abstract = {Incoherent neutron scattering by water confined in carbon
nanohorns was measured with the backscattering spectrometer
SPHERES and analyzed in exemplary breadth and depth.
Quasielastic spectra admit δ-plus-Kohlrausch fits over a
wide q and T range. From the q and T dependence of fitted
amplitudes and relaxation times, however, it becomes clear
that the fits do not represent a uniform physical process,
but that there is a crossover from localized motion at low T
to diffusive α relaxation at high T. The crossover
temperature of about 210 to 230 K increases with decreasing
wave number, which is incompatible with a thermodynamic
strong-fragile transition. Extrapolated diffusion
coefficients D(T) indicate that water motion is at room
temperature about 2.5 times slower than in the bulk; in the
supercooled state this factor becomes smaller. At even
higher temperatures, where the α spectrum is essentially
flat, a few percentages of the total scattering go into a
Lorentzian with a width of about 1.6μeV, probably due to
functional groups on the surface of the nanohorns.},
cin = {JCNS-FRM-II / Neutronenstreuung ; JCNS-1 / JCNS-2},
ddc = {530},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-1-20110106 / I:(DE-Juel1)JCNS-2-20110106},
pnm = {6215 - Soft Matter, Health and Life Sciences (POF3-621) /
6G15 - FRM II / MLZ (POF3-6G15) / 6G4 - Jülich Centre for
Neutron Research (JCNS) (POF3-623)},
pid = {G:(DE-HGF)POF3-6215 / G:(DE-HGF)POF3-6G15 /
G:(DE-HGF)POF3-6G4},
experiment = {EXP:(DE-MLZ)SPHERES-20140101 / EXP:(DE-MLZ)SCG-20150203},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000369437700004},
doi = {10.1103/PhysRevE.93.022104},
url = {https://juser.fz-juelich.de/record/281859},
}