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000283650 1001_ $$0P:(DE-HGF)0$$aMahy, Julien G.$$b0$$eCorresponding author
000283650 245__ $$aFe$^{3+}$/Iron Oxide/SiO$_{2}$ Xerogel Catalysts for p-nitrophenol Degradation by Photo-Fenton Effects: Influence of Thermal Treatment on Catalysts Texture
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000283650 520__ $$aThree iron xerogel catalysts were synthesized by hydrolysis and condensation of tetraethoxysilane (TEOS) and 3-(2-aminoethylamino)propyltrimethoxysilane (EDAS) which is able to form a chelate with iron ions. Four thermal treatments were applied to catalysts: drying, drying-autoclaving, calcination and calcination-autoclaving. Textural characterizations show that the specific surface area is increased by calcination while materials microporosity completely collapse when using autoclaving. Based on Mössbauer spectroscopy and magnetometry measurements, only Fe3+ species were observed in xerogel catalysts. The photo-Fenton effect of these catalysts was evaluated on the degradation of p-nitrophenol in aqueous media. In the presence of H2O2, results show that this effect reachs 99% of degradation after 24 h. Mössbauer and catalytic tests are presented in another paper.
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000283650 7001_ $$0P:(DE-Juel1)145213$$aHerlitschke, Marcus$$b2
000283650 7001_ $$0P:(DE-HGF)0$$aLambert, Stéphanie D.$$b3
000283650 7001_ $$0P:(DE-Juel1)130706$$aHermann, Raphael$$b4
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