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000029423 084__ $$2WoS$$aSpectroscopy
000029423 1001_ $$0P:(DE-HGF)0$$aDombovari, J.$$b0
000029423 245__ $$aICP-MS determination of trace elements in the serum samples of healthy subjects using different sample preparation methods
000029423 260__ $$aNorwalk, Conn.$$bPerkin-Elmer$$c2001
000029423 300__ $$a331- 335
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000029423 440_0 $$0701$$aAtomic Spectroscopy$$v22$$x0195-5373
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000029423 520__ $$aThe concentration of some trace elements of clinical importance was studied in blood serum samples of healthy subjects (n=19, mean age 22 +/- 4.5 years) to determine reference ranges for the healthy urban population in Eastern Hungary. A sample preparation method has been developed using closed-vessel microwave digestion with an oxidizing acid mixture (nitric acid and hydrogen peroxide) for multielemental analysis and atmospheric wet digestion with the aqueous solution of trimethyl amine (TMAH) for the measurement of aluminum. Contamination of the samples with Al was observed during acidic microwave digestion because of the chemicals used. Trace element concentrations in the samples were measured with ICP-TIS. The reference ranges obtained were (in mug/L): Al 0.98-1.74, Cr 42.8-59.3, Mn 2.27-5.05, Fe 1282-2050, Co 0.22-0.88, Ni 0.03-16.33, Cu 691-1003, Zn 591-1217, Sr 30.37-47.37, Mo 0.73-1.19, Cd 0.02-0.62, and Pb 0.02-2.70. The results were compared to the reference ranges actually used in the clinical practice, some of which are available in the literature. The effect of the applied digestion methods on the obtained individual results and average concentration ranges was also studied.
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000029423 7001_ $$0P:(DE-HGF)0$$aVarga, Z.$$b1
000029423 7001_ $$0P:(DE-Juel1)VDB2662$$aBecker, J. S.$$b2$$uFZJ
000029423 7001_ $$0P:(DE-HGF)0$$aMatyus, J.$$b3
000029423 7001_ $$0P:(DE-HGF)0$$aKakuk, G.$$b4
000029423 7001_ $$0P:(DE-HGF)0$$aPapp, L.$$b5
000029423 773__ $$0PERI:(DE-600)840758-7$$gVol. 22, p. 331- 335$$p331- 335$$q22<331- 335$$tAtomic spectroscopy$$v22$$x0195-5373$$y2001
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