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@ARTICLE{Dombovari:29423,
author = {Dombovari, J. and Varga, Z. and Becker, J. S. and Matyus,
J. and Kakuk, G. and Papp, L.},
title = {{ICP}-{MS} determination of trace elements in the serum
samples of healthy subjects using different sample
preparation methods},
journal = {Atomic spectroscopy},
volume = {22},
issn = {0195-5373},
address = {Norwalk, Conn.},
publisher = {Perkin-Elmer},
reportid = {PreJuSER-29423},
pages = {331- 335},
year = {2001},
note = {Record converted from VDB: 12.11.2012},
abstract = {The concentration of some trace elements of clinical
importance was studied in blood serum samples of healthy
subjects (n=19, mean age 22 +/- 4.5 years) to determine
reference ranges for the healthy urban population in Eastern
Hungary. A sample preparation method has been developed
using closed-vessel microwave digestion with an oxidizing
acid mixture (nitric acid and hydrogen peroxide) for
multielemental analysis and atmospheric wet digestion with
the aqueous solution of trimethyl amine (TMAH) for the
measurement of aluminum. Contamination of the samples with
Al was observed during acidic microwave digestion because of
the chemicals used. Trace element concentrations in the
samples were measured with ICP-TIS. The reference ranges
obtained were (in mug/L): Al 0.98-1.74, Cr 42.8-59.3, Mn
2.27-5.05, Fe 1282-2050, Co 0.22-0.88, Ni 0.03-16.33, Cu
691-1003, Zn 591-1217, Sr 30.37-47.37, Mo 0.73-1.19, Cd
0.02-0.62, and Pb 0.02-2.70. The results were compared to
the reference ranges actually used in the clinical practice,
some of which are available in the literature. The effect of
the applied digestion methods on the obtained individual
results and average concentration ranges was also studied.},
keywords = {J (WoSType)},
cin = {ZCH},
ddc = {530},
cid = {I:(DE-Juel1)ZCH-20090406},
pnm = {Entwicklung analytischer Verfahren},
pid = {G:(DE-Juel1)FUEK118},
shelfmark = {Spectroscopy},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000171404900001},
url = {https://juser.fz-juelich.de/record/29423},
}