001     29423
005     20180210135647.0
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037 _ _ |a PreJuSER-29423
041 _ _ |a eng
082 _ _ |a 530
084 _ _ |2 WoS
|a Spectroscopy
100 1 _ |a Dombovari, J.
|0 P:(DE-HGF)0
|b 0
245 _ _ |a ICP-MS determination of trace elements in the serum samples of healthy subjects using different sample preparation methods
260 _ _ |a Norwalk, Conn.
|b Perkin-Elmer
|c 2001
300 _ _ |a 331- 335
336 7 _ |a Journal Article
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336 7 _ |a article
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440 _ 0 |a Atomic Spectroscopy
|x 0195-5373
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|v 22
500 _ _ |a Record converted from VDB: 12.11.2012
520 _ _ |a The concentration of some trace elements of clinical importance was studied in blood serum samples of healthy subjects (n=19, mean age 22 +/- 4.5 years) to determine reference ranges for the healthy urban population in Eastern Hungary. A sample preparation method has been developed using closed-vessel microwave digestion with an oxidizing acid mixture (nitric acid and hydrogen peroxide) for multielemental analysis and atmospheric wet digestion with the aqueous solution of trimethyl amine (TMAH) for the measurement of aluminum. Contamination of the samples with Al was observed during acidic microwave digestion because of the chemicals used. Trace element concentrations in the samples were measured with ICP-TIS. The reference ranges obtained were (in mug/L): Al 0.98-1.74, Cr 42.8-59.3, Mn 2.27-5.05, Fe 1282-2050, Co 0.22-0.88, Ni 0.03-16.33, Cu 691-1003, Zn 591-1217, Sr 30.37-47.37, Mo 0.73-1.19, Cd 0.02-0.62, and Pb 0.02-2.70. The results were compared to the reference ranges actually used in the clinical practice, some of which are available in the literature. The effect of the applied digestion methods on the obtained individual results and average concentration ranges was also studied.
536 _ _ |a Entwicklung analytischer Verfahren
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588 _ _ |a Dataset connected to Web of Science
650 _ 7 |a J
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700 1 _ |a Varga, Z.
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700 1 _ |a Becker, J. S.
|0 P:(DE-Juel1)VDB2662
|b 2
|u FZJ
700 1 _ |a Matyus, J.
|0 P:(DE-HGF)0
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700 1 _ |a Kakuk, G.
|0 P:(DE-HGF)0
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700 1 _ |a Papp, L.
|0 P:(DE-HGF)0
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773 _ _ |g Vol. 22, p. 331- 335
|p 331- 335
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|t Atomic spectroscopy
|v 22
|y 2001
|x 0195-5373
909 C O |o oai:juser.fz-juelich.de:29423
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913 1 _ |k 62.10.1
|v Entwicklung analytischer Verfahren
|l Werkstoffe der Energietechnik
|b Energietechnik
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914 1 _ |y 2001
915 _ _ |0 StatID:(DE-HGF)0010
|a JCR/ISI refereed
920 1 _ |k ZCH
|l Zentralabteilung für Chemische Analysen
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|0 I:(DE-Juel1)ZCH-20090406
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981 _ _ |a I:(DE-Juel1)ZEA-3-20090406
981 _ _ |a I:(DE-Juel1)ZCH-20090406


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Marc 21