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@ARTICLE{Gnther:37136,
author = {Günther, K. and Dürbeck, H.-W. and Kleist, E. and Thiele,
B. and Prast, H. and Schwuger, J. F.},
title = {{E}ndocrine disrupting nonylphenols : ultra trace analysis
and time dependant trend in mussels from the {G}erman bight},
journal = {Fresenius' journal of analytical chemistry},
volume = {371},
issn = {0937-0633},
address = {Berlin},
publisher = {Springer},
reportid = {PreJuSER-37136},
pages = {782 - 786},
year = {2001},
note = {Record converted from VDB: 12.11.2012},
abstract = {A very sensitive and efficient analytical procedure is
presented for the determination of 4-nonylphenols (NP) in
blue mussels by use of off-line coupling of highperformance
liquid chromatography (HPLC) and gas chromatography with
mass spectrometric detection (GCMS). Combined steam
distillation and solvent extraction were used to extract the
analytes from the mussel samples. Before quantification by
GC-MS the raw extracts were purified by normal-phase HPLC.
4-n-Nonylphenol was used as internal standard. The detection
limit was 15 ng NP absolute, calculated from the blank
value. The method was applied to the determination of NP in
blue mussel samples from the German North Sea sampled over a
period of 10 years. Collection, homogenization, and storage
of the mussels were performed according to the Standard
Operating Procedures of the German Environmental Specimen
Bank since 1985. The total NP concentrations in the mussels
decreased significantly from 1985 (4 mug kg(-1)) to 1995
(1.1 mug kg(-1)).},
keywords = {J (WoSType)},
cin = {ICG-III},
ddc = {540},
cid = {I:(DE-Juel1)VDB49},
pnm = {Umweltprobenbank},
pid = {G:(DE-Juel1)FUEK84},
shelfmark = {Chemistry, Analytical},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000172508700014},
url = {https://juser.fz-juelich.de/record/37136},
}