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@ARTICLE{Zimmermann:373,
author = {Zimmermann, E. and Kemna, A. and Berwix, J. and Glaas, W.
and Münch, H. M. and Huisman, J. A.},
title = {{A} high-accuracy impedance spectrometer for measuring
sediments with low polarizability},
journal = {Measurement science and technology},
volume = {19},
issn = {0957-0233},
address = {Bristol},
publisher = {IOP Publ.},
reportid = {PreJuSER-373},
pages = {105603},
year = {2008},
note = {Record converted from VDB: 12.11.2012},
abstract = {Spectral impedance measurements are receiving increased
attention with regard to the characterization of soils,
sediments and rocks, particularly in terms of the internal
rock structure, the mineralogical composition and the
chemistry of fluids contained in porous rocks. In
fluid-saturated, porous sedimentary rocks, which are of
particular relevance for many hydrological and environmental
problems, the polarization processes that give rise to an
observed phase shift between input current and output
voltage signals are caused by the interaction of the
electrolyte in the pores of the rock with electrically
charged mineral surfaces. However, this phase response is
relatively weak, typically smaller than 10 mrad and
sometimes even of the order of only 1 mrad. In order to
reliably measure such phase responses in the relevant
frequency range, a high-accuracy impedance spectrometer is
required. This system must allow phase measurements between
1 mHz and 1 kHz with a phase accuracy better than 0.1 mrad.
In this paper, we present a new impedance spectrometer which
meets these requirements. It is based on the four-point
measurement method and offers a measurement range from 1 mHz
to 45 kHz. Furthermore, we present design information for
the sample holder and the electrodes, and methods for
performing numerical corrections to reduce measurement
errors. The overall accuracy of the setup was validated
using water and sand with well-defined polarizable objects.},
keywords = {J (WoSType)},
cin = {ICG-4 / ZEL},
ddc = {600},
cid = {I:(DE-Juel1)VDB793 / I:(DE-Juel1)ZEL-20090406},
pnm = {Terrestrische Umwelt},
pid = {G:(DE-Juel1)FUEK407},
shelfmark = {Engineering, Multidisciplinary / Instruments $\&$
Instrumentation},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000259113400021},
doi = {10.1088/0957-0233/19/10/105603},
url = {https://juser.fz-juelich.de/record/373},
}