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@ARTICLE{Schober:44537,
author = {Schober, T. and Grover Coors, W.},
title = {{E}ntry and exit of water vapor in bulk ceramic proton
conductors},
journal = {Solid state ionics},
volume = {176},
issn = {0167-2738},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {PreJuSER-44537},
pages = {357 - 362},
year = {2005},
note = {Record converted from VDB: 12.11.2012},
abstract = {An experimental study of the processes occurring during
protonation of bulk ceramic proton conductors,
BaCe0.9Y0.1O2.95 (BCY10) and BaCe0.8Y0.2O2.9 (BCY20), is
presented here. One of the faces of a disc-shaped diffusion
membrane was connected to a mass spectrometer in a vacuum
system permitting the identification of the species crossing
the ceramic-vacuum interface. Exposing the sample to D2O led
to a strong signal of D2O+ after a certain lag time. From
these lag times, the tracer diffusivity of hydrogen could be
determined as a function of temperature. The permeation of
steam consisted of two components: a fast component,
essentially given by the diffusivities of deuterons
(protons), and a slow component, ascribed to chemical
diffusion of deuterons (protons) coupled to oxygen vacancies
with the possibility of participation of even more complex
defects. Dilatometry measurements of different specimens of
BCY10 and BCY20 also revealed quite clearly this two-phase
pattern during protonation. Diffusion measurements on
protonic ceramic membranes using (H2O)-O-18 permitted the
determination of the tracer diffusivity of oxygen. All of
the above measurements were interpreted in the light of the
chemical diffusion model developed by Kreuer et al. (C) 2004
Elsevier B.V. All rights reserved.},
keywords = {J (WoSType)},
cin = {IFF-IEM},
ddc = {530},
cid = {I:(DE-Juel1)VDB321},
pnm = {Kondensierte Materie},
pid = {G:(DE-Juel1)FUEK242},
shelfmark = {Chemistry, Physical / Physics, Condensed Matter},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000226872700017},
doi = {10.1016/j.ssi.2004.07.019},
url = {https://juser.fz-juelich.de/record/44537},
}