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@ARTICLE{Stadler:4704,
author = {Stadler, A.M. and Digel, I. and Embs, J.P. and Unruh, T.
and Zaccai, G. and Büldt, G. and Artmann, G.},
title = {{F}rom {P}owder to {S}olution: {H}emoglobin {D}ynamics
{C}orrelated to {B}ody {T}emperature},
journal = {Biophysical journal},
volume = {96},
issn = {0006-3495},
address = {New York, NY},
publisher = {Rockefeller Univ. Press},
reportid = {PreJuSER-4704},
pages = {5073 - 5081},
year = {2009},
note = {This work was supported by the European Commission under
the 6th Framework Programme through the Key Action:
Strengthening the European Research Area, Research
Infrastructures (RII3-CT-2003-505925), the Institut
Laue-Langevin (M.T.), and the AINSE (M.T.).},
abstract = {A transition in hemoglobin (Hb), involving partial
unfolding and aggregation, has been shown previously by
various biophysical methods. The correlation between the
transition temperature and body temperature for Hb from
different species, suggested that it might be significant
for biological function. To focus on such biologically
relevant human Hb dynamics, we studied the protein internal
picosecond motions as a response to hydration, by elastic
and quasielastic neutron scattering. Rates of fast diffusive
motions were found to be significantly enhanced with
increasing hydration from fully hydrated powder to
concentrated Hb solution. In concentrated protein solution,
the data showed that amino acid side chains can explore
larger volumes above body temperature than expected from
normal temperature dependence. The body temperature
transition in protein dynamics was absent in fully hydrated
powder, indicating that picosecond protein dynamics
responsible for the transition is activated only at a
sufficient level of hydration. A collateral result from the
study is that fully hydrated protein powder samples do not
accurately describe all aspects of protein picosecond
dynamics that might be necessary for biological function.},
keywords = {Body Temperature / Elasticity / Hemoglobins: chemistry /
Humans / Neutrons / Powders / Solutions / Water: chemistry /
Hemoglobins (NLM Chemicals) / Powders (NLM Chemicals) /
Solutions (NLM Chemicals) / Water (NLM Chemicals) / J
(WoSType)},
cin = {ISB-2},
ddc = {570},
cid = {I:(DE-Juel1)ISB-2-20090406},
pnm = {Programm Biosoft},
pid = {G:(DE-Juel1)FUEK443},
experiment = {EXP:(DE-MLZ)TOF-TOF-20140101},
shelfmark = {Biophysics},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:19527667},
pmc = {pmc:PMC2712052},
UT = {WOS:000267194600032},
doi = {10.1016/j.bpj.2009.03.043},
url = {https://juser.fz-juelich.de/record/4704},
}