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@ARTICLE{Halder:47423,
author = {Halder, S. and Schneller, T. and Waser, R.},
title = {{C}rystallization temperature limit of ({B}a,{S}r){T}i{O}3
thin films prepared by a non oxocarbonate phase forming
{CSD} route},
journal = {Journal of sol gel science and technology},
volume = {33},
issn = {0928-0707},
address = {Dordrecht [u.a.]},
publisher = {Springer Science + Business Media B.V},
reportid = {PreJuSER-47423},
pages = {299 - 306},
year = {2005},
note = {Record converted from VDB: 12.11.2012},
abstract = {Anew chemical solution deposition (CSD) route for the
fabrication of Ba0.7Sr0.3TiO3 (BST) thin films has been
developed which completely prevents the formation of an
intermediate oxo-carbonate phase. The latter has been
reported previously by several authors to be responsible for
increased crystallization temperatures. Barium and strontium
diaminoethoxides were synthesized starting from pure barium
and strontium metal and aminoethanol. These alkoxides were
found to be readily soluble in a wide range of solvents and
thus were excellent candidates for the CSD process. To
prepare a stable precursor solution the aminoalkoxides were
dissolved in 2-butoxyethanol and then used for the
deposition of BST thin films. We conclude that the minimum
crystallization temperature of 600 degrees C to be
independent of the formation of the oxo-carbonate phase.
DTA-TGA were performed on the precursors and their solutions
to study their decomposition behaviour. All films annealed
at different temperatures were physically characterized by
XRD, IR, and SEM. The films prepared by this route at 650
degrees C were found to have high dielectric constant and
the leakage currents were comparable to BST films prepared
by normal carboxylate based routes at 750 degrees C.},
keywords = {J (WoSType)},
cin = {IFF-IEM / CNI},
ddc = {600},
cid = {I:(DE-Juel1)VDB321 / I:(DE-Juel1)VDB381},
pnm = {Kondensierte Materie},
pid = {G:(DE-Juel1)FUEK242},
shelfmark = {Materials Science, Ceramics},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000228212900006},
doi = {10.1007/s10971-005-6379-6},
url = {https://juser.fz-juelich.de/record/47423},
}