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000049348 084__ $$2WoS$$aCrystallography
000049348 1001_ $$0P:(DE-HGF)0$$aKuklin, A. I.$$b0
000049348 245__ $$aThe spacial structure of dendritic macromolecules
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000049348 440_0 $$03041$$aJournal of Applied Crystallography$$v38$$x0021-8898
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000049348 520__ $$aA low-resolution ab initio shape determination was performed from small-angle neutron and X-ray scattering (SANS and SAXS) curves from solutions of polycarbosilane dendrimers with the three-functional and the four-functional branching centre of the fourth, fifth, sixth, seventh and eighth generations. In all cases, anisometric dendrimer shapes were obtained. The overall shapes of the dendrimers with the three-and four-functional branching centres were oblate ellipsoids of revolution and triaxial ellipsoids, respectively. The restored bead models revealed a pronounced heterogeneity within the dendrimer structure. The density deficit was observed in the central part and close to the periphery of the dendrimers. The fraction of the overall volume of the dendrimers available for solvent penetration was about 0.2-0.3. These results may help in the design of new practical applications of dendrimer macromolecules.
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000049348 7001_ $$0P:(DE-HGF)0$$aOzerin, A. N.$$b1
000049348 7001_ $$0P:(DE-HGF)0$$aIslamov, A. Kh.$$b2
000049348 7001_ $$0P:(DE-HGF)0$$aMuzafarov, A. M.$$b3
000049348 7001_ $$0P:(DE-Juel1)VDB482$$aGordeliy, V. I.$$b4$$uFZJ
000049348 7001_ $$0P:(DE-HGF)0$$aRebrov, E.$$b5
000049348 7001_ $$0P:(DE-HGF)0$$aIgnateva, G. M.$$b6
000049348 7001_ $$0P:(DE-HGF)0$$aOzerina, L. A.$$b7
000049348 7001_ $$0P:(DE-HGF)0$$aTatarinova, E. A.$$b8
000049348 7001_ $$0P:(DE-Juel1)VDB58329$$aMukhametzianov, R. I.$$b9$$uFZJ
000049348 7001_ $$0P:(DE-HGF)0$$aOzerina, L. A.$$b10
000049348 7001_ $$0P:(DE-HGF)0$$aSharipov, E. Yu.$$b11
000049348 773__ $$0PERI:(DE-600)2020879-0$$a10.1107/S0021889805032115$$gVol. 38, p. 996 - 1003$$p996 - 1003$$q38<996 - 1003$$tJournal of applied crystallography$$v38$$x0021-8898$$y2005
000049348 8567_ $$uhttp://hdl.handle.net/2128/2653$$uhttp://dx.doi.org/10.1107/S0021889805032115
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