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@ARTICLE{Bode:51092,
      author       = {Bode, S. E. and Müller, M. and Wolberg, M.},
      title        = {{D}iastereomer-differentiating hydrolysis of
                      1,3-diol-acetonides : a simplified procedure for the
                      separation of syn- and anti-1,3-diols},
      journal      = {Organic letters},
      volume       = {4},
      issn         = {1523-7060},
      address      = {Washington, DC},
      publisher    = {ACS},
      reportid     = {PreJuSER-51092},
      pages        = {619 - 621},
      year         = {2002},
      note         = {Record converted from VDB: 12.11.2012},
      abstract     = {[reaction: see text] A new method to facilitate the
                      separation of diastereomeric syn- and anti-1,3-diols is
                      described. The method relies on the different hydrolysis
                      rates of the corresponding diastereomeric acetonides.
                      Treatment of a dichloromethane solution of syn- and
                      anti-1,3-diol-acetonide with a catalytic amount of diluted
                      aqueous hydrochloric acid leads to the selective cleavage of
                      the anti diastereomer. The resulting anti-1,3-diol can be
                      easily separated from the unchanged syn-1,3-diol-acetonide.},
      keywords     = {Catalysis / Dioxanes: chemical synthesis / Hydrolysis /
                      Indicators and Reagents / Kinetics / Stereoisomerism /
                      Dioxanes (NLM Chemicals) / Indicators and Reagents (NLM
                      Chemicals) / J (WoSType)},
      cin          = {IBT-2},
      ddc          = {540},
      cid          = {I:(DE-Juel1)VDB56},
      pnm          = {Biotechnologie},
      pid          = {G:(DE-Juel1)FUEK256},
      shelfmark    = {Chemistry, Organic},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {pmid:11843606},
      UT           = {WOS:000173885800038},
      doi          = {10.1021/ol017223u},
      url          = {https://juser.fz-juelich.de/record/51092},
}