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@ARTICLE{Pithan:53256,
author = {Pithan, C. and Shiratori, Y. and Waser, R. and Dornseiffer,
J. and Haegel, F.-H.},
title = {{P}reparation, processing and characterization of
nano-crystalline {B}a{T}i{O}3 powders and ceramics derived
from microemulsion mediated synthesis},
journal = {Journal of the American Ceramic Society},
volume = {0},
issn = {0002-7820},
address = {Oxford [u.a.]},
publisher = {Wiley-Blackwell},
reportid = {PreJuSER-53256},
pages = {2908},
year = {2006},
note = {Record converted from VDB: 12.11.2012},
abstract = {Monodisperse and nanocrystalline BaTiO3 powders of
different stoichiometries were synthesized through the
hydrolytic decomposition of mixed metal alkoxide solutions
with water-in-oil microemulsions as reaction media. The
method allows a tailor-made preparation of powder particles
as small as 10 nm in average. Characterization with respect
to purity, morphology, and behavior upon annealing was
conducted in order to determine appropriate processing
conditions for the preparation of pure, dense
nanocrystalline ceramics. As a result, ceramics with a mean
grain size as small as 35 nm were achieved. Raman
spectroscopy revealed for the first time local tetragonality
in pure nanocrystalline bulk BaTiO3-ceramics with such a
fine microstructure.},
cin = {IFF-IEM / ICG-II},
ddc = {660},
cid = {I:(DE-Juel1)VDB321 / I:(DE-Juel1)VDB48},
pnm = {Kondensierte Materie / Atmosphäre und Klima},
pid = {G:(DE-Juel1)FUEK414 / G:(DE-Juel1)FUEK406},
shelfmark = {Materials Science, Ceramics},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000239863100035},
doi = {10.1111/j.1551-2916.2006.01144.x},
url = {https://juser.fz-juelich.de/record/53256},
}