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@PHDTHESIS{Fischer:5438,
author = {Fischer, Sarah Christine},
title = {{K}orrosion von {PCA} durch {M}etalljodidschmelzen sowie
deren {B}enetzungseigenschaften},
volume = {44},
issn = {1866-1793},
school = {RWTH Aachen},
type = {Dr. (Univ.)},
address = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {PreJuSER-5438},
isbn = {978-3-89336-584-5},
series = {Schriften des Forschungszentrums Jülich : Energie $\&$
Umwelt / Energy $\&$ Environment},
pages = {148 S.},
year = {2009},
note = {Record converted from VDB: 12.11.2012; RWTH Aachen, Diss.,
2009},
abstract = {On high-energy discharge lamps with burners consisting of
polycrystalline aluminum oxide (PCA) corrosion leads to
relocation of the wall material; the extent of the
phenomenon depends on the composition and the wetting
behaviour of the liquid salt mixture contained in the lamp.
The aim of this work was to better comprehend these
phenomena. For this the wetting behaviours of several
iodides on PCA- and carbon plates in a water-free argon
atmosphere was determined in a contact angle measurement
apparatus. While pure salts show good or, at high
temperatures, complete wetting, the surface wetting of
binary salt mixtures is positively worse, even if only small
amounts of the second component are present. From the
contact angle measurements the surface tension of the pure
salts could be determined. By combining the
YOUNG-LAPLACE-Equation with the BUTLER-Equation, the excess
GIBBS energy could be related to the contact angles of salt
mixtures, which makes the estimation of their wetting
properties possible. The extent of the corrosion was
determined by annealing experiments in a temperature
gradient. No corrosion was found in reference experiments
without any salt. In addition to diverse corrosion phenomena
the formation of cerium aluminate was observed in some
cases. All these effects could also be reproduced by
computer simulations, for which a special program was
developed. This program may lead to the development of
advanced software in the future which can calculate the
shape and corrosivity of lamp-relevant salt melts.},
cin = {IEF-2},
cid = {I:(DE-Juel1)VDB810},
pnm = {Rationelle Energieumwandlung},
pid = {G:(DE-Juel1)FUEK402},
typ = {PUB:(DE-HGF)11 / PUB:(DE-HGF)3},
url = {https://juser.fz-juelich.de/record/5438},
}