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000000545 0247_ $$2DOI$$a10.1016/j.jmr.2009.02.010
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000000545 041__ $$aeng
000000545 082__ $$a550
000000545 084__ $$2WoS$$aBiochemical Research Methods
000000545 084__ $$2WoS$$aPhysics, Atomic, Molecular & Chemical
000000545 084__ $$2WoS$$aSpectroscopy
000000545 1001_ $$0P:(DE-HGF)0$$aBauer, C.$$b0
000000545 245__ $$aDesign of a permanent magnet with a mechanical sweep suitable for variable-temperature continuous-wave and pulsed EPR spectroscopy
000000545 260__ $$aAmsterdam [u.a.]$$bElsevier$$c2009
000000545 300__ $$a222 - 227
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000000545 440_0 $$09881$$aJournal of Magnetic Resonance$$v198$$x1090-7807$$y2
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000000545 520__ $$aA magnetic system is introduced which consists of three nested rings of permanent magnets of a Halbach dipolar layout and is capable for EPR spectroscopy. Two of the rings can be rotated independently to adjust the magnetic flux in the center and even allow for mechanical field sweeps. The presented prototype achieves a magnetic flux range of 0.0282-0.3013T with a minimal sweep of 0.15mT and homogeneity of about 10(-3). First applications with CW and pulsed Mims ENDOR as well as ESEEM experiments on a sample of a glycine single crystal doped with 1% copper nitrate demonstrate that flux range, sweep accuracy and homogeneity of this prototype is sufficient for EPR experiments on most solid samples. Together with a recently improved design magnets can be build which could serve as compact and easily transportable replacement of standard electromagnets with negligible consumption of power or coolants.
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000000545 588__ $$aDataset connected to Web of Science, Pubmed
000000545 650_2 $$2MeSH$$aElectromagnetic Fields
000000545 650_2 $$2MeSH$$aElectron Spin Resonance Spectroscopy: instrumentation
000000545 650_2 $$2MeSH$$aEquipment Design
000000545 650_2 $$2MeSH$$aGlycine: chemistry
000000545 650_2 $$2MeSH$$aMagnetics
000000545 650_2 $$2MeSH$$aMicrowaves
000000545 650_2 $$2MeSH$$aTemperature
000000545 650_7 $$056-40-6$$2NLM Chemicals$$aGlycine
000000545 650_7 $$2WoSType$$aJ
000000545 65320 $$2Author$$aESR
000000545 65320 $$2Author$$aElectron spin resonance
000000545 65320 $$2Author$$aElectron paramagnetic resonance
000000545 65320 $$2Author$$aCopper
000000545 65320 $$2Author$$aESEEM
000000545 65320 $$2Author$$aENDOR
000000545 65320 $$2Author$$aNested Halbach dipoles
000000545 7001_ $$0P:(DE-HGF)0$$aRaich, H.$$b1
000000545 7001_ $$0P:(DE-HGF)0$$aJeschke, G.$$b2
000000545 7001_ $$0P:(DE-Juel1)VDB49819$$aBlümler, P.$$b3$$uFZJ
000000545 773__ $$0PERI:(DE-600)1469665-4$$a10.1016/j.jmr.2009.02.010$$gVol. 198, p. 222 - 227$$p222 - 227$$q198<222 - 227$$tJournal of magnetic resonance$$v198$$x1090-7807$$y2009
000000545 8567_ $$uhttp://dx.doi.org/10.1016/j.jmr.2009.02.010
000000545 8564_ $$uhttps://juser.fz-juelich.de/record/545/files/FZJ-545.pdf$$yRestricted$$zPublished final document.
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000000545 9141_ $$y2009
000000545 915__ $$0StatID:(DE-HGF)0010$$aJCR/ISI refereed
000000545 9201_ $$0I:(DE-Juel1)ICG-3-20090406$$d31.10.2010$$gICG$$kICG-3$$lPhytosphäre$$x1
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