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@ARTICLE{PichardoPedrero:56024,
author = {Pichardo-Pedrero, E. and Giesen, M.},
title = {{C}omparative {STM} {S}tudies on island equilibrium shapes,
shape fluctuations and island coalescence on {A}u(001)
electrodes in chloric and sulfuric acid solutions},
journal = {Electrochimica acta},
volume = {52},
issn = {0013-4686},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {PreJuSER-56024},
pages = {5659 - 5668},
year = {2007},
note = {Record converted from VDB: 12.11.2012},
abstract = {We present scanning tunneling microscopy data on the
dynamics of monatomic high islands on gold electrodes in
different electrolytes. From a statistical analysis of the
island fluctuations around the equilibrium shape and from
the investigation of the local perimeter curvature of the
latter we determine the step line tension and the kink
energy of gold islands on an Au(0 0 1) surface as a function
of the electrode potential. We find that in chloric acid the
step line tension is smaller than for Au(0 0 1) in sulfuric
acid, however, the kink energy is much higher which leaves
us with the puzzling result that island fluctuations are
large, however, island edges are comparatively straight.
Both energies show merely a weak dependence on the electrode
potential in contrast to our previous findings in sulfuric
acid. Furthermore, by analyzing the relaxation time of
island coalescence events we determine the dominant mass
transport on the Au(0 0 1) electrode to be terrace diffusion
where the time limiting step of the migration process is the
creation of transport species at the island edge rather than
the hopping of species on the surface. This is in apparent
contradiction to previous results from island decay studies
where a diffusion limited terrace diffusion was found. All
results can be explained if one assumes that the relevant
mass transport species on Au(0 0 1) in chloride containing
electrolytes are larger (linear) structure units rather than
single adatoms. Possible candidates for these units are
Au-Cl complexes. (c) 2006 Elsevier Ltd. All rights
reserved.},
keywords = {J (WoSType)},
cin = {IBN-4},
ddc = {540},
cid = {I:(DE-Juel1)VDB802},
pnm = {Kondensierte Materie},
pid = {G:(DE-Juel1)FUEK414},
shelfmark = {Electrochemistry},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000246655300018},
doi = {10.1016/j.electacta.2006.10.061},
url = {https://juser.fz-juelich.de/record/56024},
}