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000057170 0247_ $$2DOI$$a10.1016/j.jmmm.2006.02.103
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000057170 041__ $$aeng
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000057170 084__ $$2WoS$$aMaterials Science, Multidisciplinary
000057170 084__ $$2WoS$$aPhysics, Condensed Matter
000057170 1001_ $$0P:(DE-HGF)0$$aGroudeva-Zotova, S.$$b0
000057170 245__ $$aPhase composition and magnetic characteristics of Fe-filled multi-walled carbon nanotubes
000057170 260__ $$aAmsterdam$$bNorth-Holland Publ. Co.$$c2006
000057170 300__ $$a40 - 50
000057170 3367_ $$0PUB:(DE-HGF)16$$2PUB:(DE-HGF)$$aJournal Article
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000057170 440_0 $$03490$$aJournal of Magnetism and Magnetic Materials$$v306$$x0304-8853$$y1
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000057170 520__ $$aThe work addresses the correlation between the phase composition and the magnetic characteristics of aligned Fe-filled multi-walled carbon nanotubes (Fe-MWCNTs) grown by pyrolysis of ferrocene on oxidized Si substrates. In a combinatorial approach we exploited the extremely high gradients of the technological parameters temperature and ferrocene flow across the surface of a substrate positioned close to the reactor wall to obtain a large variation in the structural and magnetic properties of the Fe-MWCNTs. In this way, we established several clear correlations between the Fe-filling phase composition and the overall magnetic characteristics of the aligned Fe-MWCNTs. The alpha-Fe rich samples, which possess a more ordered graphitic sheet structure, a higher degree of preferred crystalline orientation of the metal filling and much larger metal crystallites in comparison with the carbide-rich samples, show a much stronger magnetic anisotropy with easy axis perpendicular to the substrate and unusually high values of the coercive field H-c and the saturation field H-s. The changes in the measured saturation magnetisation M-s and the H-c values correlate well with the variation of the alpha-Fe content and the filling crystallinity. A special annealing treatment of the samples causes a distinct increase of the alpha-Fe quantity and an increase of the measured average grain size. The respective magnetic characteristics show a significant increase of the overall magnetic moment and decrease of the coercive field. The correlation between the structural and the magnetic characteristics of the annealed samples matches quite well the respective correlations in the case of as-deposited samples. (C) 2006 Elsevier B.V. All rights reserved.
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000057170 65320 $$2Author$$amagnetic fibres
000057170 65320 $$2Author$$acrystal structure
000057170 65320 $$2Author$$aferromagnetism
000057170 65320 $$2Author$$auniaxial anisotropy
000057170 7001_ $$0P:(DE-HGF)0$$aKozhuharova, R.$$b1
000057170 7001_ $$0P:(DE-HGF)0$$aElefant, D.$$b2
000057170 7001_ $$0P:(DE-HGF)0$$aMühl, T.$$b3
000057170 7001_ $$0P:(DE-Juel1)130948$$aSchneider, C. M.$$b4$$uFZJ
000057170 7001_ $$0P:(DE-HGF)0$$aMönch, I.$$b5
000057170 773__ $$0PERI:(DE-600)1479000-2$$a10.1016/j.jmmm.2006.02.103$$gVol. 306, p. 40 - 50$$p40 - 50$$q306<40 - 50$$tJournal of magnetism and magnetic materials$$v306$$x0304-8853$$y2006
000057170 8567_ $$uhttp://dx.doi.org/10.1016/j.jmmm.2006.02.103
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000057170 915__ $$0StatID:(DE-HGF)0010$$aJCR/ISI refereed
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