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@ARTICLE{Stingaciu:5798,
author = {Stingaciu, L.-R. and Pohlmeier, A. and Blümler, P. and
Weihermüller, L. and van Dusschoten, D. and Stapf, S. and
Vereecken, H.},
title = {{C}haracterization of unsaturated porous media by
high-field and low-field {NMR} relaxometry},
journal = {Water resources research},
volume = {45},
issn = {0043-1397},
address = {Washington, DC},
publisher = {AGU},
reportid = {PreJuSER-5798},
pages = {W08412},
year = {2009},
note = {Many thanks to Y. Q. Song (Schlumberger-Doll Research,
Connecticut) for giving us access to his software for
inverse Laplace transform. The DFG (projects PO 746/2-1 and
Transregional Collaborative Research Centre 32) has to be
acknowledged for financial support and Norbert Klitzsch and
Oliver Mohnke (Applied Geophysics, RWTH Aachen University)
for providing access to the low field setup. Finally, the
reviewers are acknowledged for their very useful comments
that helped greatly with the improvement of our paper.},
abstract = {A comparison study of nuclear magnetic resonance
relaxometry at high and low magnetic field (7 and 0.1 T) has
been initiated for investigating the influence of the
magnetic field strength, variable clay content, and
different degrees of saturation on the relaxometric
properties of four ideal porous media. The samples consisted
of medium sand with increasing fractions of kaolin clay
ranging from 0 to $15\%.$ Six different volumetric water
contents between saturation and theta = 0.05 were used.
Changes in water content of the samples were achieved by
slow evaporation. T-2 relaxation curves were monitored by
the Carr-Purcell-Meiboom-Gill sequence and were further
analyzed by inverse Laplace transformation, yielding T-2
distribution functions. Sand shows a slight continuous shift
with decreasing water content of a bimodal distribution
function of T-2 to faster relaxation at high and low
magnetic field. Sand-clay mixtures show broad, bimodal
distribution functions for both magnetic field intensities
which shift slightly with decreasing water content. Signal
amplitude behavior with variation of saturation degree was
also monitored. An expected proportionality of the total
signal amplitude with water content was observed for all
samples at 0.1 T, whereas at 7 T deviations occurred for
samples with a clay content higher than $5\%,$ which are
assigned to loss of signal in the first echo periods. The
relaxivity in unsaturated clay-based porous media is mostly
surface dominated, as the weak and comparable dependence of
1/T-2 on T-E at both field strengths shows. Nevertheless,
for a reliable determination of water content in mixed
systems with varying texture and saturation the employment
of multiecho sequences at low magnetic field strength are
preferable.},
keywords = {J (WoSType)},
cin = {ICG-4 / ICG-3},
ddc = {550},
cid = {I:(DE-Juel1)VDB793 / I:(DE-Juel1)ICG-3-20090406},
pnm = {Terrestrische Umwelt},
pid = {G:(DE-Juel1)FUEK407},
shelfmark = {Environmental Sciences / Limnology / Water Resources},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000269036900002},
doi = {10.1029/2008WR007459},
url = {https://juser.fz-juelich.de/record/5798},
}