%0 Journal Article
%A Kahle, S.
%A Nussbaum, W.
%A Hehn, M.
%A Raich, H.P.
%A Wilhelm, M.
%A Blümler, P.
%T Combination of NMR relaxometry and mechanical testing during vulcanization
%J Kautschuk, Gummi, Kunststoffe
%V 3
%@ 0022-9520
%C Heidelberg
%I Hüthig
%M PreJuSER-58777
%P 92 - 94
%D 2008
%Z Record converted from VDB: 12.11.2012
%X A new design for an in-situ combination of NMR and rheological measurements is presented. The NMR instrumentation is based on a Bruker Minispec spectrometer with a home-built magnet system consisting of 64 permanent magnets in a so-called MANDHALA arrangement. This magnet reaches a flux density of about 0.23 T, corresponding to a H-1 NMR resonance frequency of about 9.5 MHz. The NMR apparatus is combined with a Scarabaeus SISV50 instrument with modified sample cells to allow synchronous in-situ rheological and NMR measurements. This unique instrument and first exemplary measurements of a curing epoxy resin and the vulcanization of a rubber sample are presented.
%K J (WoSType)
%F PUB:(DE-HGF)16
%9 Journal Article
%U <Go to ISI:>//WOS:000254117700002
%U https://juser.fz-juelich.de/record/58777