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Copyright: Hüthig: diese Version ist abrufbar unter http://imperia.mi-verlag.de/imperia/md/content/ai/pv/fachartikel/kg/2008/03/kg08_03_092.pdf
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000058777 084__ $$2WoS$$aEngineering, Chemical
000058777 084__ $$2WoS$$aPolymer Science
000058777 1001_ $$0P:(DE-HGF)0$$aKahle, S.$$b0
000058777 245__ $$aCombination of NMR relaxometry and mechanical testing during vulcanization
000058777 260__ $$aHeidelberg$$bHüthig$$c2008
000058777 300__ $$a92 - 94
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000058777 520__ $$aA new design for an in-situ combination of NMR and rheological measurements is presented. The NMR instrumentation is based on a Bruker Minispec spectrometer with a home-built magnet system consisting of 64 permanent magnets in a so-called MANDHALA arrangement. This magnet reaches a flux density of about 0.23 T, corresponding to a H-1 NMR resonance frequency of about 9.5 MHz. The NMR apparatus is combined with a Scarabaeus SISV50 instrument with modified sample cells to allow synchronous in-situ rheological and NMR measurements. This unique instrument and first exemplary measurements of a curing epoxy resin and the vulcanization of a rubber sample are presented.
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000058777 65320 $$2Author$$arheology
000058777 65320 $$2Author$$acuring
000058777 65320 $$2Author$$across-linking
000058777 65320 $$2Author$$amolecular mobility
000058777 65320 $$2Author$$apermanent magnets
000058777 65320 $$2Author$$arubber
000058777 65320 $$2Author$$aNMR
000058777 7001_ $$0P:(DE-HGF)0$$aNussbaum, W.$$b1
000058777 7001_ $$0P:(DE-HGF)0$$aHehn, M.$$b2
000058777 7001_ $$0P:(DE-HGF)0$$aRaich, H.P.$$b3
000058777 7001_ $$0P:(DE-HGF)0$$aWilhelm, M.$$b4
000058777 7001_ $$0P:(DE-Juel1)VDB49819$$aBlümler, P.$$b5$$uFZJ
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