TY  - JOUR
AU  - Kahle, S.
AU  - Nussbaum, W.
AU  - Hehn, M.
AU  - Raich, H.P.
AU  - Wilhelm, M.
AU  - Blümler, P.
TI  - Combination of NMR relaxometry and mechanical testing during vulcanization
JO  - Kautschuk, Gummi, Kunststoffe
VL  - 3
SN  - 0022-9520
CY  - Heidelberg
PB  - Hüthig
M1  - PreJuSER-58777
SP  - 92 - 94
PY  - 2008
N1  - Record converted from VDB: 12.11.2012
AB  - A new design for an in-situ combination of NMR and rheological measurements is presented. The NMR instrumentation is based on a Bruker Minispec spectrometer with a home-built magnet system consisting of 64 permanent magnets in a so-called MANDHALA arrangement. This magnet reaches a flux density of about 0.23 T, corresponding to a H-1 NMR resonance frequency of about 9.5 MHz. The NMR apparatus is combined with a Scarabaeus SISV50 instrument with modified sample cells to allow synchronous in-situ rheological and NMR measurements. This unique instrument and first exemplary measurements of a curing epoxy resin and the vulcanization of a rubber sample are presented.
KW  - J (WoSType)
LB  - PUB:(DE-HGF)16
UR  - <Go to ISI:>//WOS:000254117700002
UR  - https://juser.fz-juelich.de/record/58777
ER  -