Hauptseite > Publikationsdatenbank > Combination of NMR relaxometry and mechanical testing during vulcanization > print

001     58777
005     20200423204531.0
017 _ _ |a Mit freundlicher Genehmigung vom Hüthig-Verlag, Copyright: Hüthig: diese Version ist abrufbar unter http://imperia.mi-verlag.de/imperia/md/content/ai/pv/fachartikel/kg/2008/03/kg08_03_092.pdf
024 7 _ |a WOS:000254117700002
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037 _ _ |a PreJuSER-58777
041 _ _ |a eng
082 _ _ |a 670
084 _ _ |2 WoS
|a Engineering, Chemical
084 _ _ |2 WoS
|a Polymer Science
100 1 _ |a Kahle, S.
|b 0
|0 P:(DE-HGF)0
245 _ _ |a Combination of NMR relaxometry and mechanical testing during vulcanization
260 _ _ |a Heidelberg
|b Hüthig
|c 2008
300 _ _ |a 92 - 94
336 7 _ |a Journal Article
|0 PUB:(DE-HGF)16
|2 PUB:(DE-HGF)
336 7 _ |a Output Types/Journal article
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336 7 _ |a Journal Article
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336 7 _ |a ARTICLE
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336 7 _ |a JOURNAL_ARTICLE
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336 7 _ |a article
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440 _ 0 |a KGK Kautschuk Gummi Kunststoffe
|x 0022-9520
|0 13103
|v 3
500 _ _ |a Record converted from VDB: 12.11.2012
520 _ _ |a A new design for an in-situ combination of NMR and rheological measurements is presented. The NMR instrumentation is based on a Bruker Minispec spectrometer with a home-built magnet system consisting of 64 permanent magnets in a so-called MANDHALA arrangement. This magnet reaches a flux density of about 0.23 T, corresponding to a H-1 NMR resonance frequency of about 9.5 MHz. The NMR apparatus is combined with a Scarabaeus SISV50 instrument with modified sample cells to allow synchronous in-situ rheological and NMR measurements. This unique instrument and first exemplary measurements of a curing epoxy resin and the vulcanization of a rubber sample are presented.
536 _ _ |a Terrestrische Umwelt
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653 2 0 |2 Author
|a rheology
653 2 0 |2 Author
|a curing
653 2 0 |2 Author
|a cross-linking
653 2 0 |2 Author
|a molecular mobility
653 2 0 |2 Author
|a permanent magnets
653 2 0 |2 Author
|a rubber
653 2 0 |2 Author
|a NMR
700 1 _ |a Nussbaum, W.
|b 1
|0 P:(DE-HGF)0
700 1 _ |a Hehn, M.
|b 2
|0 P:(DE-HGF)0
700 1 _ |a Raich, H.P.
|b 3
|0 P:(DE-HGF)0
700 1 _ |a Wilhelm, M.
|b 4
|0 P:(DE-HGF)0
700 1 _ |a Blümler, P.
|b 5
|u FZJ
|0 P:(DE-Juel1)VDB49819
773 _ _ |g Vol. 3, p. 92 - 94
|p 92 - 94
|q 3<92 - 94
|0 PERI:(DE-600)542050-7
|t Kautschuk, Gummi, Kunststoffe
|v 3
|y 2008
|x 0022-9520
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914 1 _ |y 2008
915 _ _ |0 StatID:(DE-HGF)0010
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920 1 _ |k ICG-3
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|d 31.10.2010
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