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000062554 0247_ $$2DOI$$a10.1016/j.jnoncrysol.2008.03.048
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000062554 084__ $$2WoS$$aMaterials Science, Ceramics
000062554 084__ $$2WoS$$aMaterials Science, Multidisciplinary
000062554 1001_ $$0P:(DE-Juel1)VDB57378$$aVan der Donk, G. J. W.$$b0$$uFZJ
000062554 245__ $$aMicroporous and mesoporous 8YSZ materials derived from polymeric acetylacetone-modified precursors for inorganic membrane applications
000062554 260__ $$aAmsterdam [u.a.]$$bElsevier Science$$c2008
000062554 300__ $$a3723 - 3731
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000062554 440_0 $$03611$$aJournal of Non-Crystalline Solids$$v354$$x0022-3093
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000062554 520__ $$aBoth microporous and mesoporous 8% mol-yttria-stabilized zirconia (8YSZ) material can be prepared from the same 8YSZ sols. Stable 8YSZ sols with particle sizes smaller than 10 nm were prepared by using acetylacetone as a precursor modifier in combination with carboxylic acids. Nonanic and caproic acids are preferred due to their higher stability in combinations of highly concentrated sols. Cubic 8YSZ microporous material can be prepared by using acetylacetone as a precursor modifier with caproic acid as the catalyst. These materials can be transformed into mesoporous material composed of crystalline primary cubic YSZ nanoparticles by simply mixing with structure-directing agents. Use of the block copolymer F127 resulted in the largest specific surface area of 100 m(2)/g. Thin 8YSZ layers of these sols can be prepared on glass slips and on graded porous alumina supports with thicknesses between 20 and 100 nm. (C) 2008 Elsevier B.V. All rights reserved.
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000062554 65320 $$2Author$$acrystal growth
000062554 65320 $$2Author$$anucleation
000062554 65320 $$2Author$$ananocrystals
000062554 65320 $$2Author$$aspin coating
000062554 65320 $$2Author$$ascanning electron microscopy
000062554 65320 $$2Author$$amicrocrystallinity
000062554 65320 $$2Author$$acolloids
000062554 65320 $$2Author$$anano-composites
000062554 65320 $$2Author$$asolution chemistry
000062554 7001_ $$0P:(DE-Juel1)VDB55636$$aSerra, J. M.$$b1$$uFZJ
000062554 7001_ $$0P:(DE-Juel1)129637$$aMeulenberg, W. A.$$b2$$uFZJ
000062554 773__ $$0PERI:(DE-600)1500501-x$$a10.1016/j.jnoncrysol.2008.03.048$$gVol. 354, p. 3723 - 3731$$p3723 - 3731$$q354<3723 - 3731$$tJournal of non-crystalline solids$$v354$$x0022-3093$$y2008
000062554 8567_ $$uhttp://dx.doi.org/10.1016/j.jnoncrysol.2008.03.048
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