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@ARTICLE{Serra:62814,
author = {Serra, J. M. and Vert, V. B. and Büchler, O. and
Meulenberg, W. A. and Buchkremer, H. P.},
title = {{IT}-{SOFC} supported on {M}ixed {O}xygen
{I}onic-{E}lectronic {C}onducting {C}omposites},
journal = {Chemistry of materials},
volume = {20},
issn = {0897-4756},
address = {Washington, DC},
publisher = {American Chemical Society},
reportid = {PreJuSER-62814},
pages = {3867 - 3875},
year = {2008},
note = {Record converted from VDB: 12.11.2012},
abstract = {Thin oxygen-ion-conducting films (5-10 mu m) were prepared
and characterized on mixed-conducting porous substrates.
When this film is made of a pure ionic conductor, such as a
gadolinia-doped ceria (Ce0.8Gd0.2O1.9) electrolyte material,
the assembly can be used as a cathode-supported solid oxide
fuel cell (SOFC) for operation at intermediate temperatures
(500-600 degrees C). In this case, a porous anode comprising
a Ni-CGO cermet or a Pt coating is deposited on top of the
highly conductive electrolyte. Another structure with
promising applications is created when the supported
gastight layer includes a mixed conductor such as ferrite or
cobaltite perovskites acting as oxygen-permeable membrane,
which can be applied in the combustion of fuel with pure
oxygen or in the intensification of other industrial
processes currently using aerial catalytic oxidation. The
different supported films and multilayer assemblies were
characterized by SEM, EDS-WDX, SIMS, helium, and oxygen
permeation, showing that gastight thin films can be achieved
(values >1 x 10(-6) mbar L s(-1) cm(-2)) by inexpensive
coating procedures (screen-printing or slip-casting). The
electrochemical properties of thin CGO electrolytes were
studied by impedance spectroscopy (EIS) and DC voltammetry
on fully assembled fuel cells. It is concluded that thin CGO
electrolytes under hydrogen atmosphere have enough n-type
electronic conductivity to reduce the cell potential by
$5-20\%$ from the Nernst potential, which causes the
consequent power density decrease. A possible solution to
these leakage currents is the use of a thin
electron-blocking layer as stabilized zirconia (YSZ or SSZ)
deposited on the fuel-exposed CGO electrolyte side. Oxygen
permeation of thin LSFC layers was measured using air and
helium (sweep) in the range from 700 to 1000 degrees C.
Supported thin films exhibit much better permeation fluxes
than bulk thick membranes, especially when oxygen-reduction
catalytic porous coatings were applied.},
keywords = {J (WoSType)},
cin = {IEF-1},
ddc = {540},
cid = {I:(DE-Juel1)VDB809},
pnm = {Rationelle Energieumwandlung / SOFC - Solid Oxide Fuel Cell
(SOFC-20140602)},
pid = {G:(DE-Juel1)FUEK402 / G:(DE-Juel1)SOFC-20140602},
shelfmark = {Chemistry, Physical / Materials Science, Multidisciplinary},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000256854800016},
doi = {10.1021/cm702508f},
url = {https://juser.fz-juelich.de/record/62814},
}