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@ARTICLE{Yoon:6491,
author = {Yoon, S. and Dornseiffer, J. and Schneller, T. and Henning,
D. and Iwaya, S. and Pithan, C. and Waser, R.},
title = {{P}ercolative {B}a{T}i{O}3-{N}i composite nanopowders from
alkoxide-mediated synthesis},
journal = {Journal of the European Ceramic Society},
volume = {30},
issn = {0955-2219},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {PreJuSER-6491},
pages = {561 - 567},
year = {2010},
note = {Record converted from VDB: 12.11.2012},
abstract = {BaTiO3-Ni nanopowders have been synthesized via an
alkoxide-mediated synthesis route through the hydrolysis and
condensation of barium hydroxide octahydrate and titanium
(IV) isopropoxide in the presence of submicron sized,
spherical Ni particles originating from a commercial Ni
paste, that was introduced during the preparation procedure.
X-ray diffraction (XRD) patterns indicate that nanocomposite
powders of the phases BaTiO3 and Ni could be successfully
prepared and tailor-made composition control was confirmed.
Scanning electron microscopy (SEM) and transmission electron
microscopy (TEM) show that the synthesized BaTiO3
nanoparticles were aggregates of nanosized primary particles
as small as 40 nm in diameter. The average Ni particle size
was estimated to be about 200 turn. Dilatometric
measurements on green compacts of these powders revealed
that the shrinkage of BaTiO3-Ni composites is retarded
compared to both, pure BaTiO3 and Ni. Thermogravimetric
analysis (TGA) shows weight losses due to the decomposition
of organic binder from Ni paste, the release of water from
the surface and of hydroxyl ions from inside the lattice of
the BaTiO3 nanoparticles. With the addition of nickel, the
dielectric constant increased slightly due to the
percolation effect. (C) 2009 Elsevier Ltd. All rights
reserved.},
keywords = {J (WoSType)},
cin = {IFF-6 / JARA-FIT / ICG-2},
ddc = {660},
cid = {I:(DE-Juel1)VDB786 / $I:(DE-82)080009_20140620$ /
I:(DE-Juel1)VDB791},
pnm = {Grundlagen für zukünftige Informationstechnologien /
Atmosphäre und Klima},
pid = {G:(DE-Juel1)FUEK412 / G:(DE-Juel1)FUEK406},
shelfmark = {Materials Science, Ceramics},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000272455600077},
doi = {10.1016/j.jeurceramsoc.2009.06.024},
url = {https://juser.fz-juelich.de/record/6491},
}