TY - JOUR AU - Matusch, A. AU - Depboylu, C. AU - Palm, C. AU - Wu, B. AU - Höglinger, G.U. AU - Schäfer, M.K.-H. AU - Becker, J. S. TI - Cerebral Bioimaing of Cu, Fe, Zn, and Mn in the MPTP Mouse Model of Parkinson&#8217;s Disease Using Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) JO - Journal of the American Society for Mass Spectrometry VL - 21 SN - 1044-0305 CY - New York [u.a.] PB - Springer M1 - PreJuSER-7995 SP - 161 - 171 PY - 2010 N1 - The authors thank A. Zimmermann (Forschungszentrum Julich) for technical support with LA-ICP-MS measurements. This study was supported in part by the German Parkinson's Society and the University Hospitals of Giessen and Marburg, Germany. AB - Laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) has been established as a powerful technique for the determination of metal and nonmetal distributions within biological systems with high sensitivity. An imaging LA-ICP-MS technique for Fe, Cu, Zn, and Mn was developed to produce large series of quantitative element maps in native brain sections of mice subchronically intoxicated with 1-methyl-4-phenyl-1,2,3,6-tetrahydropyridin (MPTP) as a model of Parkinson's disease. Images were calibrated using matrix-matched laboratory standards. A software solution allowing a precise delineation of anatomical structures was implemented. Coronal brain sections were analyzed crossing the striatum and the substantia nigra, respectively. Animals sacrificed 2 h, 7 d, or 28 d after the last MPTP injection and controls were investigated. We observed significant decreases of Cu concentrations in the periventricular zone and the fascia dentata at 2 h and 7d and a recovery or overcompensation at 28 d, most pronounced in the rostral periventricular zone (+40%). In the cortex Cu decreased slightly to -10%. Fe increased in the interpeduncular nucleus (+40%) but not in the substantia nigra. This pattern is in line with a differential regulation of periventricular and parenchymal Cu, and with the histochemical localization of Fe, and congruent to regions of preferential MPTP binding described in the rodent brain. The LA-ICP-MS technique yielded valid and statistically robust results in the present study on 39 slices from 19 animals. Our findings underline the value of routine micro-local analytical techniques in the life sciences and affirm a role of Cu availability in Parkinson's disease. KW - 1-Methyl-4-phenyl-1,2,3,6-tetrahydropyridine: pharmacology KW - Animals KW - Brain: drug effects KW - Brain: pathology KW - Brain Chemistry KW - Calibration KW - Copper: analysis KW - Equipment Design KW - Iron: analysis KW - Laser Therapy KW - Male KW - Manganese: analysis KW - Mass Spectrometry: instrumentation KW - Mass Spectrometry: methods KW - Metals, Heavy: analysis KW - Mice KW - Mice, Inbred C57BL KW - Neurotoxins: pharmacology KW - Parkinson Disease: metabolism KW - Zinc: analysis KW - Metals, Heavy (NLM Chemicals) KW - Neurotoxins (NLM Chemicals) KW - 1-Methyl-4-phenyl-1,2,3,6-tetrahydropyridine (NLM Chemicals) KW - Iron (NLM Chemicals) KW - Manganese (NLM Chemicals) KW - Copper (NLM Chemicals) KW - Zinc (NLM Chemicals) KW - J (WoSType) LB - PUB:(DE-HGF)16 C6 - pmid:19892565 UR - <Go to ISI:>//WOS:000274518100021 DO - DOI:10.1016/j.jasms.2009.09.022 UR - https://juser.fz-juelich.de/record/7995 ER -