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000807731 1001_ $$0P:(DE-HGF)0$$aGrzechnik, Andrzej$$b0$$eCorresponding author
000807731 245__ $$aHigh-pressure behaviour of Cs$_{2}$V$_{3}$O$_{8}$ fresnoite
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000807731 520__ $$aCrystal structure of Cs2V3O8 fresnoite (P4bm, Z=2) has been studied using single-crystal X-ray diffraction in a diamond anvil cell to 8.6 GPa at room temperature. Cs2V3O8 undergoes a reversible first-order phase transition at about 4 GPa associated with anomalies in the pressure dependencies of the lattice parameters and unit-cell volume but without any symmetry change. Both structures consist of layers of corner-sharing V5+O4 tetrahedra and V4+O5 tetragonal pyramids separated by the Cs+ cations located between the layers. At low pressures, the compression has little effect on the polarity of the structure. Above 4 GPa, the pseudosymmetry with respect to the corresponding centrosymmetric space group P4/mbm abruptly increases. The effects of external pressure and of the A+ cation substitution in the vanadate fresnoites A2V3O8 (A+: K+, Rb+, NH4+, Cs+) are discussed
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000807731 7001_ $$0P:(DE-HGF)0$$aZur Loye, Hans-Conrad$$b2
000807731 7001_ $$0P:(DE-Juel1)145694$$aFriese, Karen$$b3
000807731 773__ $$0PERI:(DE-600)1469806-7$$a10.1016/j.jssc.2016.03.041$$gVol. 238, p. 252 - 258$$p252 - 258$$tJournal of solid state chemistry$$v238$$x0022-4596$$y2016
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