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@ARTICLE{Beltramo:8081,
author = {Beltramo, G. L. and Giesen, M. and Ibach, H.},
title = {{A}nomalous {H}elmholtz-{C}apacitance on {S}tepped
{S}urfaces of {S}ilver and {G}old},
journal = {Electrochimica acta},
volume = {54},
issn = {0013-4686},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {PreJuSER-8081},
pages = {4305 - 4311},
year = {2009},
note = {We thank Karina Morgenstern, University Hannover, for a
helpful exchange of ideas on the adsorption of water at
steps and for making STM images available to us prior to
publication. Inspiring discussions with Wolfgang Schmickler,
University Ulm, are also gratefully acknowledged. Udo Linke
has contributed significantly to this work by his careful
and innovative preparation of the crystal surfaces. The work
was partially supported by the Fond derChemischen Industrie
and the Deutsche Forschungsgemeinschaft.},
abstract = {We have studied the capacitance of the solid/electrolyte
interface on Ag(11n) and Au(11n) surfaces in KClO4 and HClO4
as function of the electrolyte concentration and the step
density. We find that the inner layer capacitance
(Helmholtz-capacitance) at the potential of (total) zero
charge is dramatically reduced on stepped surfaces. Standard
theories which describe the Helmholtz-capacitance by
properties of the liquid, a hard wall boundary condition and
the polarizability of the electron gas at the metal surface
fail to describe this behavior. We propose that the
different polarizability of water bonded to the surface need
be taken into account and attribute the reduced capacitance
at steps to the lower polarizability of water molecules
bonded to step edges. (C) 2009 Elsevier Ltd. All rights
reserved.},
keywords = {J (WoSType)},
cin = {IBN-3 / JARA-FIT / IBN-4},
ddc = {540},
cid = {I:(DE-Juel1)VDB801 / $I:(DE-82)080009_20140620$ /
I:(DE-Juel1)VDB802},
pnm = {Grundlagen für zukünftige Informationstechnologien /
Kondensierte Materie},
pid = {G:(DE-Juel1)FUEK412 / G:(DE-Juel1)FUEK414},
shelfmark = {Electrochemistry},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000266826200004},
doi = {10.1016/j.electacta.2009.02.087},
url = {https://juser.fz-juelich.de/record/8081},
}