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@ARTICLE{Niemller:810837,
      author       = {Niemöller, Arvid and Jakes, Peter and Kayser, Steffen and
                      Lin, Yu and Lehnert, Werner and Granwehr, Josef},
      title        = {3{D} printed sample holder for in-operando {EPR}
                      spectroscopy on high temperature polymer electrolyte fuel
                      cells},
      journal      = {Journal of magnetic resonance},
      volume       = {269},
      issn         = {1090-7807},
      address      = {Amsterdam [u.a.]},
      publisher    = {Elsevier},
      reportid     = {FZJ-2016-03420},
      pages        = {157 - 161},
      year         = {2016},
      abstract     = {Electrochemical cells contain electrically conductive
                      components, which causes various problems if such a cell is
                      analyzed during operation in an EPR resonator. The optimum
                      cell design strongly depends on the application and it is
                      necessary to make certain compromises that need to be
                      individually arranged. Rapid prototyping presents a
                      straightforward option to implement a variable cell design
                      that can be easily adapted to changing requirements. In this
                      communication, it is demonstrated that sample containers
                      produced by 3D printing are suitable for EPR applications,
                      with a particular emphasis on electrochemical applications.
                      The housing of a high temperature polymer electrolyte fuel
                      cell (HT-PEFC) with a phosphoric acid doped
                      polybenzimidazole membrane was prepared from polycarbonate
                      by 3D printing. Using a custom glass Dewar, this fuel cell
                      could be operated at temperatures up to 140 °C in a
                      standard EPR cavity. The carbon-based gas diffusion layer
                      showed an EPR signal with a characteristic Dysonian line
                      shape, whose evolution could be monitored in-operando in a
                      non-invasive manner.},
      cin          = {IEK-9 / IEK-3},
      ddc          = {550},
      cid          = {I:(DE-Juel1)IEK-9-20110218 / I:(DE-Juel1)IEK-3-20101013},
      pnm          = {131 - Electrochemical Storage (POF3-131) / HITEC -
                      Helmholtz Interdisciplinary Doctoral Training in Energy and
                      Climate Research (HITEC) (HITEC-20170406)},
      pid          = {G:(DE-HGF)POF3-131 / G:(DE-Juel1)HITEC-20170406},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000381239900019},
      pubmed       = {pmid:27323280},
      doi          = {10.1016/j.jmr.2016.06.003},
      url          = {https://juser.fz-juelich.de/record/810837},
}