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000811504 0247_ $$2doi$$a10.1039/C6NR03776C
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000811504 0247_ $$2ISSN$$a2040-3372
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000811504 1001_ $$0P:(DE-HGF)0$$aWetterskog, Erik$$b0$$eCorresponding author
000811504 245__ $$aTuning the structure and habit of iron oxide mesocrystals
000811504 260__ $$aCambridge$$bRSC Publ.$$c2016
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000811504 520__ $$aA precise control over the meso- and microstructure of ordered and aligned nanoparticle assemblies, i.e., mesocrystals, is essential in the quest for exploiting the collective material properties for potential applications. In this work, we produced evaporation-induced self-assembled mesocrystals with different mesostructures and crystal habits based on iron oxide nanocubes by varying the nanocube size and shape and by applying magnetic fields. A full 3D characterization of the mesocrystals was performed using image analysis, high-resolution scanning electron microscopy and Grazing Incidence Small Angle X-ray Scattering (GISAXS). This enabled the structural determination of e.g. multi-domain mesocrystals with complex crystal habits and the quantification of interparticle distances with sub-nm precision. Mesocrystals of small nanocubes (l = 8.6–12.6 nm) are isostructural with a body centred tetragonal (bct) lattice whereas assemblies of the largest nanocubes in this study (l = 13.6 nm) additionally form a simple cubic (sc) lattice. The mesocrystal habit can be tuned from a square, hexagonal to star-like and pillar shapes depending on the particle size and shape and the strength of the applied magnetic field. Finally, we outline a qualitative phase diagram of the evaporation-induced self-assembled superparamagnetic iron oxide nanocube mesocrystals based on nanocube edge length and magnetic field strength.
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000811504 7001_ $$0P:(DE-Juel1)144041$$aKlapper, Alice$$b1
000811504 7001_ $$0P:(DE-HGF)0$$aDisch, Sabrina$$b2
000811504 7001_ $$0P:(DE-Juel1)130742$$aJosten, Elisabeth$$b3
000811504 7001_ $$0P:(DE-Juel1)130928$$aRücker, Ulrich$$b4
000811504 7001_ $$0P:(DE-Juel1)130572$$aBrückel, Thomas$$b5
000811504 7001_ $$0P:(DE-HGF)0$$aBergström, Lennart$$b6
000811504 7001_ $$0P:(DE-HGF)0$$aSalazar-Alvarez, German$$b7$$eCorresponding author
000811504 7001_ $$0P:(DE-Juel1)130706$$aHermann, Raphael$$b8
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