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024 7 _ |a 10.1039/C6NR03776C
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024 7 _ |a 2040-3364
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024 7 _ |a 2040-3372
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024 7 _ |a 2128/12211
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037 _ _ |a FZJ-2016-03961
041 _ _ |a English
082 _ _ |a 600
100 1 _ |a Wetterskog, Erik
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245 _ _ |a Tuning the structure and habit of iron oxide mesocrystals
260 _ _ |a Cambridge
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520 _ _ |a A precise control over the meso- and microstructure of ordered and aligned nanoparticle assemblies, i.e., mesocrystals, is essential in the quest for exploiting the collective material properties for potential applications. In this work, we produced evaporation-induced self-assembled mesocrystals with different mesostructures and crystal habits based on iron oxide nanocubes by varying the nanocube size and shape and by applying magnetic fields. A full 3D characterization of the mesocrystals was performed using image analysis, high-resolution scanning electron microscopy and Grazing Incidence Small Angle X-ray Scattering (GISAXS). This enabled the structural determination of e.g. multi-domain mesocrystals with complex crystal habits and the quantification of interparticle distances with sub-nm precision. Mesocrystals of small nanocubes (l = 8.6–12.6 nm) are isostructural with a body centred tetragonal (bct) lattice whereas assemblies of the largest nanocubes in this study (l = 13.6 nm) additionally form a simple cubic (sc) lattice. The mesocrystal habit can be tuned from a square, hexagonal to star-like and pillar shapes depending on the particle size and shape and the strength of the applied magnetic field. Finally, we outline a qualitative phase diagram of the evaporation-induced self-assembled superparamagnetic iron oxide nanocube mesocrystals based on nanocube edge length and magnetic field strength.
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700 1 _ |a Bergström, Lennart
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700 1 _ |a Salazar-Alvarez, German
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700 1 _ |a Hermann, Raphael
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