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@ARTICLE{BenitoAbascal:817670,
author = {Benito Abascal, M. and Bläsing, Marc and Ninomiya, Y. and
Müller, Michael},
title = {{I}nfluence of {S}team, {H}ydrogen {C}hloride and
{H}ydrogen {S}ulphide on the {R}elease and {C}ondensation of
{Z}inc in {G}asification},
journal = {Industrial $\&$ engineering chemistry research},
volume = {55},
number = {25},
issn = {0888-5885},
address = {Columbus, Ohio},
publisher = {American Chemical Society},
reportid = {FZJ-2016-04338},
pages = {6911–6921},
year = {2016},
abstract = {The aim of this work was to assess the influence of H2O,
HCl, and H2S on the condensation and release of zinc. The
condensation behavior of the zinc vapors was investigated in
a heated flow channel reactor housed in a furnace with a gas
cooling zone, where eight glass filters were placed on
different cooling stages. The metal species deposited in the
filters were determined by means of ion chromatography (IC)
and inductively coupled plasma optical emission spectroscopy
(ICP-OES). Experiments on the release of the inorganic
vapors were carried out in a heated flow channel reactor
coupled to a molecular beam mass spectrometer (MBMS). The
experiments were carried out under two typical gasification
conditions (H2/H2O/He or Ar) and atmospheric pressure with
50 and 500 ppmv of HCl and H2S. Hot gas analysis was done at
900, 800, 700, and 500 °C. The condensation experiments
showed that zinc condensed as ZnO, ZnCl2, and ZnS under the
conditions considered. The species detected in the gas phase
were Zn, ZnO, ZnCl2, and ZnS. The experimental results were
compared with Scheil–Gulliver cooling calculations carried
out with FactSage 6.3 software. This model was proven to be
an excellent tool for the prediction of the behavior of zinc
under gasification conditions. Furthermore, the global
kinetics of the condensation experiments was clarified with
the thermodynamic pseudoequilibrium model recently developed
by researchers of Chubu University (Japan). With this work,
not only a good understanding of the behavior of the zinc
under gasification conditions was obtained, but also the
finding and evidence of a powerful tool for predicting fast
and easily the behavior of trace metals under gasification
conditions.},
cin = {IEK-2},
ddc = {540},
cid = {I:(DE-Juel1)IEK-2-20101013},
pnm = {111 - Efficient and Flexible Power Plants (POF3-111)},
pid = {G:(DE-HGF)POF3-111},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000378984600003},
doi = {10.1021/acs.iecr.6b01637},
url = {https://juser.fz-juelich.de/record/817670},
}