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@PHDTHESIS{Zhang:819606,
author = {Zhang, Jing},
title = {{S}orption of polycyclic aromatic hydrocarbon ({PAH}) to
{Y}angtze {R}iver sediments and their components},
volume = {59},
school = {RWTH Aachen},
type = {Dr.},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2016-05227},
isbn = {978-3-89336-616-3},
series = {Schriften des Forschungszentrums Jülich Reihe Energie $\&$
Umwelt / Energy $\&$ Environment},
pages = {X, 109},
year = {2010},
note = {RWTH Aachen, Diss., 2010},
abstract = {Sorption of hydrophobic organic chemical (HOC) to natural
sediments includescomplex mechanisms. The present work
studies the sorption of polycyclic aromatichydrocarbon (PAH)
to Yangtze River sediments. The major objectives were
toinvestigate the sorption mechanisms of PAH to sediments
and the effect of sedimentsheterogeneity. Specifically, the
sorption and distribution of PAH in the fractions
ofamorphous organic carbon (AOC), black carbon (BC) and
mineral surface wereinvestigated. Pyrene and phenanthrene
were involved as major target PAH chemicals for examining
the sorption equilibriums in single and binary solute
systems. The sorbents include model sediment constituents
and five sediments collected from the Yangtze River. The
preheated sediments according to the chemothermal oxidation
method (CTO-375, Gustafsson et al., 1997) were also studied.
In which, the remaining organic carbon (OC)is considered as
BC. Analytical procedures for the determination of PAH in
solution were developed with fluorescence spectroscopy.
Especially, the synchronous fluorescence spectroscopy (SFS)
was applied for simultaneous analyses of the primary solute
and cosolute PAH in binary solute systems. The sorption
isotherms were fitted with different types of model,
including Freundlich model, Polanyi-based adsorption model
and composite models which comprise a partition model and an
adsorption model. The major findings include the following
aspects. Firstly, the sorption of pyrene to pristine
sediments was found to be mainly dependent on the OC content
rather than on the specific surface area (SSA) or the
microporosity of sorbents. Composite models were applied for
distinguishing the partition and adsorption. The adsorption
dominates in the low concentration range, while the
partition becomesmore important at high concentrations. The
fitted partition coefficients are linearly dependent on the
AOC content (fAOC) of sediments, which supports a pyrene
partition in the AOC phase in sediments at a high
equilibrium concentration. Secondly, the fitted adsorption
of pyrene to pristine sediments was compared with that to
the preheated sediments. Our finding that the adsorption
capacity of the BC fraction is similar in pristine and
preheated sediments suggests that the low content AOC in the
pristine sediments does not affect the adsorption capacity
of the BC fraction. However, variations of fitting
parameters suppose that the adsorption dynamics may be
alteredthrough dispersive or flocculating effect. A
distribution model of pyrene between the AOC, BC and mineral
fractions of sediment was established according to the
fitted results with model and natural sorbents. It was found
that the adsorption to BC dominates the overall sorption at
low concentrations (relative concentration C$_{r}$ < 0.1).
The contribution of AOC becomes more important at high
concentrations. In the presence of OC in sediments, the
contribution of the mineral fraction to the overall sorption
is negligible.},
cin = {IBG-3},
cid = {I:(DE-Juel1)IBG-3-20101118},
pnm = {899 - ohne Topic (POF3-899)},
pid = {G:(DE-HGF)POF3-899},
typ = {PUB:(DE-HGF)3 / PUB:(DE-HGF)11},
url = {https://juser.fz-juelich.de/record/819606},
}