TY - JOUR
AU - Kovacic, Filip
AU - Bleffert, Florian
AU - Caliskan, Muttalip
AU - Wilhelm, Susanne
AU - Granzin, Joachim
AU - Batra-Safferling, Renu
AU - Jaeger, Karl-Erich
TI - A membrane-bound esterase PA2949 from Pseudomonas aeruginosa is expressed and purified from Escherichia coli
JO - FEBS Open Bio
VL - 6
IS - 5
SN - 2211-5463
CY - Cambridge
PB - Elsevier on behalf of the Federation of European Biochemical Societies
M1 - FZJ-2016-06319
SP - 484 - 493
PY - 2016
AB - Pseudomonas aeruginosa strain 1001 produces an esterase (EstA) that can hydrolyse the racemic methyl ester of b-acetylthioisobutyrate to produce the (D)-enantiomer, which serves as a precursor of captopril, a drug used for treatment of hypertension. We show here that PA2949 from P. aeruginosa PA01, a homologue of EstA, can efficiently be expressed in an enzymatically active form in E. coli. The enzyme is membrane-associated as demonstrated by cell fractionation studies. PA2949 was purified to homogeneity after solubilisation with the nonionic detergent, Triton X-100, and was shown to possess a conserved esterase catalytic triad consisting of Ser137–His258–Asp286. Our results should allow the development of an expression and purification strategy to produce this biotechnologically relevant esterase in a pure form with a high yield.
LB - PUB:(DE-HGF)16
UR - <Go to ISI:>//WOS:000375915100012
C6 - pmid:27419054
DO - DOI:10.1002/2211-5463.12061
UR - https://juser.fz-juelich.de/record/821075
ER -