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@ARTICLE{Shi:823944,
author = {Shi, Jie and Cao, Xinyun and Chen, Yaozong and Cronan, John
E. and Guo, Zhihong},
title = {{A}n {A}typical α/β-{H}ydrolase {F}old {R}evealed in the
{C}rystal {S}tructure of {P}imeloyl-{A}cyl {C}arrier
{P}rotein {M}ethyl {E}sterase {B}io{G} from {H}aemophilus
influenzae},
journal = {Biochemistry},
volume = {55},
issn = {1520-4995},
address = {Columbus, Ohio},
publisher = {American Chemical Society},
reportid = {FZJ-2016-06572},
pages = {6705-6717},
year = {2016},
abstract = {Pimeloyl-acyl carrier protein (ACP) methyl esterase is an
α/β-hydrolase that catalyzes the last biosynthetic step of
pimeloyl-ACP, a key intermediate in biotin biosynthesis.
Intriguingly, multiple nonhomologous isofunctional forms of
this enzyme that lack significant sequence identity are
present in diverse bacteria. One such esterase, Escherichia
coli BioH, has been shown to be a typical α/β-hydrolase
fold enzyme. To gain further insights into the role of this
step in biotin biosynthesis, we have determined the crystal
structure of another widely distributed pimeloyl-ACP methyl
esterase, Haemophilus inf luenzae BioG, at 1.26 Å. The BioG
structure is similar to the BioH structure and is composed
of an α-helical lid domain and a core domain that contains
a central sevenstranded β-pleated sheet. However, four of
the six α-helices that flank both sides of the BioH core
β-sheet are replaced with long loops in BioG, thus forming
an unusual α/β-hydrolase fold. This structural variation
results in a significantly decreased thermal stability of
the enzyme. Nevertheless, the lid domain and the residues at
the lid−core interface are well conserved between BioH and
BioG, in which an analogous hydrophobic pocket for pimelate
binding as well as similar ionic interactions with the ACP
moiety are retained. Biochemical characterization of
sitedirected mutants of the residues hypothesized to
interact with the ACP moiety supports a similar substrate
interaction mode for the two enzymes. Consequently, these
enzymes package the identical catalytic function under a
considerably different protein surface.},
cin = {ICS-6},
ddc = {570},
cid = {I:(DE-Juel1)ICS-6-20110106},
pnm = {553 - Physical Basis of Diseases (POF3-553)},
pid = {G:(DE-HGF)POF3-553},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000389557300012},
doi = {10.1021/acs.biochem.6b00818},
url = {https://juser.fz-juelich.de/record/823944},
}