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@ARTICLE{Bick:824445,
author = {Bick, D. S. and Kindsmüller, A. and Staikov, G. and
Gunkel, F. and Müller, D. and Schneller, T. and Waser, R.
and Valov, Ilia},
title = {{S}tability and {D}egradation of {P}erovskite
{E}lectrocatalysts for {O}xygen {E}volution {R}eaction},
journal = {Electrochimica acta},
volume = {218},
issn = {0013-4686},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2016-07034},
pages = {156 - 162},
year = {2016},
abstract = {Pr0.2Ba0.8CoO3-δ (PBCO) and Ba0.5Sr0.5Co0.5Fe0.5O3-δ
(BSCF) perovskite thin film electrodes were used as model
systems for testing degradation and stability during oxygen
evolution reaction (OER) in alkaline water electrolysis. The
catalyst films were prepared by chemical solution deposition
(CSD) and are binder-free. Stepwise aging experiments
illustrate a systematical approach to different degrees of
degradation of the perovskites after defined testing cycles
of cyclic voltammetry in application-near conditions. XPS
and EDX characterization at each aging step enables a
monitoring of the change in chemical composition during
degradation. XPS analysis points to a change in the defect
chemistry of PBCO during degradation. The influence of all
monitored parameters on the overall electrode service
lifetime is shown in a novel end of service life test (ESLT)
at thin film perovskite electrodes of 100 nm thickness.},
cin = {PGI-6 / PGI-7},
ddc = {540},
cid = {I:(DE-Juel1)PGI-6-20110106 / I:(DE-Juel1)PGI-7-20110106},
pnm = {521 - Controlling Electron Charge-Based Phenomena
(POF3-521)},
pid = {G:(DE-HGF)POF3-521},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000385840100021},
doi = {10.1016/j.electacta.2016.09.116},
url = {https://juser.fz-juelich.de/record/824445},
}