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@ARTICLE{Pillai:824682,
author = {Pillai, Rishi and Chyrkin, Anton and Grüner, Daniel and
Nowak, Wojciech and Zheng, N. and Kliewe, A. and Quadakkers,
Willem J.},
title = {{C}arbides in an {A}luminised {S}ingle {C}rystal
{S}uperalloy: {T}rancing the {S}ource of {C}arbon},
journal = {Surface and coatings technology},
volume = {288},
issn = {0257-8972},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2016-07240},
pages = {15-24},
year = {2016},
abstract = {Single crystal Ni-base superalloys contain marginal amounts
of carbon and as a consequence, diffusion coatings on these
superalloys are generally expected to result in carbide free
interdiffusion zones (IDZ) containing intermetallic
precipitates. The experimentally observed presence of
carbides in the IDZ of the aluminised (CVD) single crystal
SC2000 led to a thorough investigation of the source of
carbon as well as the precipitate phases occurring in the
coating and in the IDZ. Scanning electron microscopy (SEM)
combined with energy- and wavelength-dispersive X-ray
spectroscopy (EDX/WDX) was employed to characterise the
aluminised superalloy specimens. Average concentration
profiles were determined by glow discharge optical emission
spectroscopy (GDOES). Phases were then identified by X-Ray
diffraction (XRD) and electron backscatter diffraction
(EBSD). The carbides in the interdiffusion zone were found
to be of the type M6C/M12C. By aluminising specimens of
SC2000 with different thicknesses, the available carbon
reservoir for the precipitation of carbides was varied. The
amount of carbides in the IDZ after coating decreased with
decreasing thickness of the substrate specimen. Hence it
could be confirmed that carbon indeed diffused from the
substrate to the coating/substrate interface and did not
originate from the service environment.},
cin = {IEK-2},
ddc = {620},
cid = {I:(DE-Juel1)IEK-2-20101013},
pnm = {111 - Efficient and Flexible Power Plants (POF3-111)},
pid = {G:(DE-HGF)POF3-111},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000371549200003},
doi = {10.1016/j.surfcoat.2015.12.066},
url = {https://juser.fz-juelich.de/record/824682},
}