% IMPORTANT: The following is UTF-8 encoded. This means that in the presence
% of non-ASCII characters, it will not work with BibTeX 0.99 or older.
% Instead, you should use an up-to-date BibTeX implementation like “bibtex8” or
% “biber”.
@ARTICLE{Finkeldei:824857,
author = {Finkeldei, S. and Kegler, Ph. and Kowalski, Piotr and
Schreinemachers, C. and Brandt, F. and Bukaemskiy, Andrey
and Vinograd, Victor and Beridze, G. and Shelyug, A. and
Navrotsky, A. and Bosbach, D.},
title = {{C}omposition dependent order-disorder transition in
{N}d$_{x}${Z}r$_{1−x}${O}$_{2−0.5x}$ pyrochlores: {A}
combined structural, calorimetric and ab initio modeling
study},
journal = {Acta materialia},
volume = {125},
issn = {1359-6454},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2016-07359},
pages = {166 - 176},
year = {2017},
abstract = {The order-disorder phase transition in the
NdxZr1−xO2−0.5x system is studied by complementary
techniques which include wet chemical synthesis of a series
of compositions with various Nd/Zr ratios with the final
annealing at 1873 K, X-ray diffraction, oxide melt solution
calorimetry and ab initio thermodynamic modeling. Our
structural data indicate the transition from ordered to
disordered pyrochlore at x ∼0.31 at a temperature of 1873
K. Our calorimetric data show a transition enthalpy of ∼30
kJ/mol, which corresponds to an entropy of disordering of
∼16 J/K/mol. The latter value is significantly smaller
than the configurational entropy of transition computed
under the assumption of complete disorder in a fluorite
phase, indicating a substantial degree of order remaining in
the fluorite phase at the temperature of synthesis. The
considered phases are computed ab initio using a series of
special quasi-random structures that emulate the complete or
partial disorder. The results of our calculations and
thermodynamic modeling are in good agreement with the
measured lattice parameters, the Nd content at the
order-disorder transition, and the measured formation and
transformation enthalpies. Thus our combined experimental
and modeling results provide valuable insight into the
disordering of this pyrochlore phase and of other pyrochlore
materials.},
cin = {IEK-6 / JARA-HPC},
ddc = {670},
cid = {I:(DE-Juel1)IEK-6-20101013 / $I:(DE-82)080012_20140620$},
pnm = {161 - Nuclear Waste Management (POF3-161) / Investigation
of the new materials for safe management of high level
nuclear waste. $(jiek61_20131101)$ / Investigation of the
new materials for safe management of high level nuclear
waste. $(jara0038_20121101)$ / Towards controlled QCD
transport coefficients $(jara0039_20121101)$},
pid = {G:(DE-HGF)POF3-161 / $G:(DE-Juel1)jiek61_20131101$ /
$G:(DE-Juel1)jara0038_20121101$ /
$G:(DE-Juel1)jara0039_20121101$},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000394201500015},
doi = {10.1016/j.actamat.2016.11.059},
url = {https://juser.fz-juelich.de/record/824857},
}