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| 100 | 1 | _ | |a Krapf, Philipp |0 P:(DE-Juel1)169356 |b 0 |u fzj |
| 245 | _ | _ | |a Seyferth-Gilbert Homologation as a Route to 18 F-Labeled Building Blocks: Preparation of Radiofluorinated Phenylacetylenes and Their Application in PET Chemistry |
| 260 | _ | _ | |a Weinheim |c 2016 |b Wiley-VCH Verl. |
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| 520 | _ | _ | |a A convenient method for the preparation of hitherto unknown ([F-18]fluorophenyl)acetylenes ([F-18]FPAs) using the Seyferth-Gilbert homologation is reported. The novel building blocks were efficiently prepared from easily accessible [F-18]fluorobenzaldehydes by using the Bestmann-Ohira reagent. High radiochemical yields and excellent radiochemical purities were achieved within only 20 min of reaction time; 2- and 4-[F-18]FPAs were applied to prepare radiofluorinated heterocycles by using different cycloaddition and cross-coupling reactions. Additionally, these building blocks were used to prepare three novel PET tracers. Thus, an artificial radiofluorinated protected amino acid [F-18]10, a COX-2-specific ligand [F-18]14, and a PSMA-selective inhibitor [F-18]16 were obtained in high radiochemical yields. |
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| 773 | _ | _ | |a 10.1002/ejoc.201501377 |g Vol. 2016, no. 3, p. 430 - 433 |0 PERI:(DE-600)1475010-7 |n 3 |p 430 - 433 |t European journal of organic chemistry |v 2016 |y 2016 |x 1434-193X |
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