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@ARTICLE{Falkenstein:826300,
author = {Falkenstein, Andreas and Müller, David and De Souza, Roger
A. and Martin, Manfred},
title = {{C}hemical relaxation experiments on mixed conducting
oxides with large stoichiometry deviations},
journal = {Solid state ionics},
volume = {280},
issn = {0167-2738},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2017-00533},
pages = {66 - 73},
year = {2015},
abstract = {Relaxation techniques are widely used to determine the mass
transport parameters of oxygen, namely the chemical surface
exchange coefficient kchem and the chemical diffusion
coefficient Dchem, of mixed ionic-electronic conductors. The
investigation of technologically relevant mixed conducting
oxides that exhibit high values of both kchem and Dchem by
relaxation methods faces the problem that the amount of
oxygen released or taken up by the sample during a
relaxation experiment is not negligible. In fact, it can be
of the same order as the amount supplied by the gas stream;
the desired step-like change in oxygen activity that
initiates the relaxation process thus becomes ill defined.
In this study we examine strategies to identify and
counteract this problem: As a model system we use the mixed
ionic electronic conducting perovskite-type oxide
Ba0.5Sr0.5Co0.8Fe0.2O3 − δ, which exhibits
extraordinarily high oxygen exchange kinetics, and we
perform conductivity relaxation experiments that monitor the
oxygen partial pressure in the vicinity of the sample.},
cin = {PGI-6},
ddc = {530},
cid = {I:(DE-Juel1)PGI-6-20110106},
pnm = {522 - Controlling Spin-Based Phenomena (POF3-522)},
pid = {G:(DE-HGF)POF3-522},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000362605500009},
doi = {10.1016/j.ssi.2015.07.023},
url = {https://juser.fz-juelich.de/record/826300},
}