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@ARTICLE{Wang:826554,
author = {Wang, Wei and ma, peixiang and Dong, Hui and Krause,
Hans-Joachim and Zhang, Yi and Willbold, Dieter and
Offenhäusser, Andreas and Gu, Zhongwei},
title = {{A} magnetic nanoparticles relaxation sensor for
protein-protein interaction detection at ultra-low magnetic
field},
journal = {Biosensors and bioelectronics},
volume = {80},
issn = {0956-5663},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2017-00773},
pages = {661–665},
year = {2016},
abstract = {Functionalized magnetic nanoparticles (MNPs) can serve as
magnetic relaxation sensors (MRSs) to detect different
biological targets, because the clustering of magnetic
particle may cause the spin-spin relaxation time (T2)
decrease of the surrounding water protons. However, the
application of MNPs in clinical NMR systems faces the
challenge of poor stability at magnetic field strengths in
the order of tesla. The recently developed ultra-low field
(ULF) NMR technique working at microtesla (μT) range then
becomes a candidate. Herein, we incorporated superconducting
quantum interference device (SQUID) as the detector in the
ultra-low field system to enhance the sensitivity. We
functionalized the Fe3O4 nanoparticles with the
gama-aminobutyrate type A receptor-associated proteins
(GABARAP), which specifically interact with calreticulin
(CRT). As a result of the interaction between GABARAP and
CRT, the clustering of the functionalized MNPs generates
local magnetic fields, which accelerate the dephasing of the
water protons in the vicinity. We analyzed the relation
between T2 values and the CRT concentrations at 211μT and
the low detection limit for CRT is 10 pg/ml, which is
superior to the immunoblot system. The high sensitivity of
the ULF NMR system for protein-protein interaction detection
demonstrates the potential to use this inexpensive, portable
system for quick biochemical and clinical assays.},
cin = {ICS-6},
ddc = {570},
cid = {I:(DE-Juel1)ICS-6-20110106},
pnm = {551 - Functional Macromolecules and Complexes (POF3-551)},
pid = {G:(DE-HGF)POF3-551},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000372558500091},
doi = {10.1016/j.bios.2016.02.037},
url = {https://juser.fz-juelich.de/record/826554},
}