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@ARTICLE{Jeangros:827061,
      author       = {Jeangros, Q. and Hansen, T. and Wagner, J. B. and
                      Dunin-Borkowski, Rafal and Hébert, C. and van Herle, J. and
                      Hessler - Wyser, A.},
      title        = {{E}nergy-filtered environmental transmission electron
                      microscopy for the assessment of solid-gas reactions at
                      elevated temperature:{N}i{O}/{YSZ}-{H}$_{2}$ as a case
                      study},
      journal      = {Ultramicroscopy},
      volume       = {169},
      issn         = {0304-3991},
      address      = {Amsterdam},
      publisher    = {Elsevier Science},
      reportid     = {FZJ-2017-01267},
      pages        = {11 -21},
      year         = {2016},
      abstract     = {A novel approach, which is based on the analysis of
                      sequences of images recorded using energy-filtered
                      transmission electron microscopy and can be used to assess
                      the reaction of a solid with a gas at elevated temperature,
                      is illustrated for the reduction of a NiO/ceramic solid
                      oxide fuel cell anode in 1.3 mbar of H2. Three-window
                      elemental maps and jump-ratio images of the O K edge and
                      total inelastic mean free path images are recorded as a
                      function of temperature and used to provide local and
                      quantitative information about the reaction kinetics and the
                      volume changes that result from the reaction. Under certain
                      assumptions, the speed of progression of the reaction front
                      in all three dimensions is obtained, thereby providing a
                      three-dimensional understanding of the reaction.},
      cin          = {PGI-5 / ER-C-1},
      ddc          = {570},
      cid          = {I:(DE-Juel1)PGI-5-20110106 / I:(DE-Juel1)ER-C-1-20170209},
      pnm          = {143 - Controlling Configuration-Based Phenomena (POF3-143)},
      pid          = {G:(DE-HGF)POF3-143},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000383819100002},
      pubmed       = {pmid:27421078},
      doi          = {10.1016/j.ultramic.2016.06.005},
      url          = {https://juser.fz-juelich.de/record/827061},
}