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000828196 1001_ $$0P:(DE-Juel1)166483$$aZischler, Johannes$$b0
000828196 245__ $$aAlcohol-Enhanced Cu-Mediated Radiofluorination
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000828196 520__ $$aThe potential of many 18F-labeled (hetero)aromatics for applications in positron emission tomography remains underexplored because convenient procedures for their radiosynthesis are lacking. Consequently, simple methods to prepare radiofluorinated (hetero)arenes are highly sought after. Herein, we report the beneficial effect of primary and secondary alcohols on Cu-mediated 18F-labeling. This observation contradicts the assumption that such alcohols are inappropriate solvents for aromatic fluorination. Therefore, we developed a protocol for rapid radiolabeling of an extraordinarily broad scope of boronic and stannyl substrates under general reaction conditions. Notably, radiofluorinated indoles, phenols, and anilines were synthesized directly from the corresponding unprotected precursors. Furthermore, the novel method enabled the preparation of radiofluorinated tryptophans, [18F]F-DPA, [18F]DAA1106, 6-[18F]FDA, and 6-[18F]FDOPA
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000828196 7001_ $$0P:(DE-HGF)0$$aKolks, Niklas$$b1
000828196 7001_ $$0P:(DE-Juel1)162416$$aModemann, Daniel$$b2$$ufzj
000828196 7001_ $$0P:(DE-Juel1)166419$$aNeumaier, Bernd$$b3$$eCorresponding author
000828196 7001_ $$0P:(DE-HGF)0$$aZlatopolskiy, Boris D.$$b4
000828196 773__ $$0PERI:(DE-600)1478547-x$$a10.1002/chem.201604633$$gVol. 23, no. 14, p. 3251 - 3256$$n14$$p3251 - 3256$$tChemistry - a European journal$$v23$$x0947-6539$$y2017
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