TY  - JOUR
AU  - Schmitz, Paulo
AU  - Jakelski, Rene
AU  - Jalkanen, Kirsi
AU  - Winter, Martin
AU  - Bieker, Peter
TI  - Synthesis of High-Purity Imidazolium Tetrafluoroborates and Bis(oxalato)borates
JO  - Chemistry - a European journal
VL  - 23
IS  - 10
SN  - 0947-6539
CY  - Weinheim
PB  - Wiley-VCH
M1  - FZJ-2017-02791
SP  - 2261 - 2264
PY  - 2017
AB  - The synthesis and purification of imidazolium-based ionic liquids (ILs) with boron-containing anions is reported. The scope was the optimization of the meta thesis reaction and on the purification of the synthesized ILs. It was possible to reduce the reaction and purification times, to avoid the use of acetonitrile as processing solvent, and to increase the yield compared to the known procedure for [BOB]− anion-containing ILs. Furthermore, to the best of our knowledge the flashpoints of the ILs could be determined for the first time by the continuously closed-cup flashpoint (CCCFP) method.
LB  - PUB:(DE-HGF)16
UR  - <Go to ISI:>//WOS:000395583200004
C6  - pmid:28112849
DO  - DOI:10.1002/chem.201604461
UR  - https://juser.fz-juelich.de/record/828974
ER  -