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@ARTICLE{Meister:829001,
author = {Meister, Paul and Schmuelling, Guido and Winter, Martin and
Placke, Tobias},
title = {{N}ew insights into the uptake/release of {FTFSI} −
anions into graphite by means of in situ powder {X}-ray
diffraction},
journal = {Electrochemistry communications},
volume = {71},
issn = {1388-2481},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2017-02818},
pages = {52 - 55},
year = {2016},
abstract = {The redox-amphoteric character of graphite enables its
utilization as intercalation host for various types of
cations and anions to form either donor-type or
acceptor-type graphite intercalation compounds (GICs),
respectively. While the donor-type GIC LiC6 is commonly used
in the field of lithium ion batteries, acceptor-type GICs
were suggested for application in dual-ion cells. In this
contribution, the electrochemical
intercalation/de-intercalation of
fluorosulfonyl-(trifluoromethanesulfonyl) imide (FTFSI−)
anions into graphite was studied for dual-ion cells during a
cyclic voltammetry experiment using in situ powder X-ray
diffraction. For the GICs, a series of most dominant stages
could be assigned and the periodic repeat distance as well
as the FTFSI− gallery height/gallery expansion were
determined. The obtained dominant stage numbers of the
formed GICs were correlated to cell voltage ranges. Upon
charge, a transition of the different stages was observed,
while upon discharge stage 1 was still preserved for a broad
voltage range. These novel findings indicate different
mechanisms for the uptake and release of the anions.},
cin = {IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000383445000012},
doi = {10.1016/j.elecom.2016.08.003},
url = {https://juser.fz-juelich.de/record/829001},
}