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@PHDTHESIS{Skaja:834335,
author = {Skaja, Katharina},
title = {{R}edox processes and ionic transport in resistive
switching binary metal oxides},
volume = {49},
school = {RWTH Aachen},
type = {Dr.},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2017-04310},
isbn = {978-3-95806-236-8},
series = {Schriften des Forschungszentrums Jülich. Reihe Information
/ Information},
pages = {VII, 203 S.},
year = {2017},
note = {RWTH Aachen, Diss., 2016},
abstract = {The growing demand for non-volatile memories requires new
concepts in data storage and mobile computing, as the
existing flash technology runs into a physical scaling
limit. One of the promising candidates for future
non-volatile memories is Redox-based Resistive Random Access
Memory (ReRAM). This memory technology is based on a
non-volatile and reversible switching of device resistance
with an external stimulus. The reversible resistance change
in the memristive device can be attributed to an electro
reduction, which takes place in the metal oxide and/or at
the metal oxide electrode interface. The formation of ionic
defects and their motion are involved in the electrically
induced redox processes, which for most metal oxides is
correlated to a valence change of metal ions. Within this
thesis the microscopic processes in memristive devices are
investigated in order to understand the defect configuration
and defect motion in metal oxide thin films. Furthermore,
the redox processes localized in nanoscale filaments induced
by field-driven defect motion has been elucidated. The
resistive switching characteristic of Ta$_{2}$O$_{5-x}$
single layers as well as Nb$_{2}$O$_{5-x}$/
Ta$_{2}$O$_{5-x}$ heterostructures has been investigated. It
could be demonstrated that the forming voltage of the
memristive devices can be modified by different reactive
sputtering conditions. During electrical biasing a
morphological change with a dendrite-like shape occurs at
the top electrode. The formation of this dendrite-like
structure at the metal oxide/metal interface, has been
correlated to an avalanche discharge induced redox process
in the metal oxide. The dendrite-like structure can be
assigned to an oxygen deficient amorphous phase of the metal
oxide. The predominant defects in TiO$_{2-x}$ are determined
by ionic charge compensation at intermediate oxygen partial
pressure and dominated by electronic charge compensation at
reducing conditions. For Ta$_{2}$O$_{5-x}$ ceramics as well
as thin films the electrical conductivity is dominated by
ionic charge compensation over the entire investigated
oxygen partial pressure range. The formation energy for
oxygen vacancies of single crystal/ceramics is comparable to
the values of the thin films. At oxidizing conditions the
thin films show an enhanced ionic conduction due to an
increased concentration of defects at the grain boundaries
and an accumulation of the space charges. The equilibration
process in TiO$_{2-x}$ single crystals as well as in thin
films is dominated by a surface exchange process. The
velocity of the equilibration process is influenced by the
surface orientation of single crystals. In TiO$_{2-x}$ thin
films a two-fold surface exchange process has been
identified. As origin of this two-fold process the
incorporation or release of a second species such as water
was discussed as well as the influence of the texturing of
the thin film and the influence of the substrate.},
cin = {PGI-7},
cid = {I:(DE-Juel1)PGI-7-20110106},
pnm = {521 - Controlling Electron Charge-Based Phenomena
(POF3-521)},
pid = {G:(DE-HGF)POF3-521},
typ = {PUB:(DE-HGF)3 / PUB:(DE-HGF)11},
url = {https://juser.fz-juelich.de/record/834335},
}