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@INPROCEEDINGS{Ferraresi:834447,
author = {Ferraresi, Giulio and Kazzi, Mario El and Tsai, Chih-Long
and Uhlenbruck, Sven and Novák, Petr and Villevieille,
Claire},
title = {{A}lloy-based electrodes for all-solid-state {L}i-ion
batteries based on garnet {T}a-substituted
{L}i7{L}a3{Z}r2{O}12 solid electrolyte},
reportid = {FZJ-2017-04403},
year = {2017},
abstract = {Since the dawn of Li-ion batteries, consumers have always
been concerned about the safety of the electronic devices.
Recent accidents (Samsung S7 Galaxy Note and Boeing 787
Dreamliner aircraft) have pushed to look for alternatives to
liquid electrolytes considered to be the main risk for the
low safety of the battery. Solid electrolytes are envisaged
as alternative of organic liquid electrolytes since they
promise to improve safety at both room and elevated
temperatures. Among the already discovered inorganic Li-ion
conductors, the garnet material with a cubic structure,
Li7La3Zr2O12 (LLZO), offers both acceptable ionic
conductivity at room temperature and chemical stability in
contact with Li metal.1Generally, such solid electrolyte is
often investigated in half-cells (vs. Li metal) coupled to
oxide materials such as Li4Ti5O12 or LiCoO2 as negative and
positive electrode, respectively. Although the garnet solid
electrolyte (LLZO) was considered to be stable in the
potential range from zero to six volt vs. Li/Li+, recent
studies point out that the stability window could be
drastically limited down to 2.9 V.2We investigated the
electrochemical performance of alloy-based (Sn, Si)
nanoparticles as electrode using a Ta-doped LLZO pellet as
solid electrolyte to build all-solid-state Li half-cells.
Alloy materials are known to be electrochemically active in
the range 0-1.5 V vs. Li/Li+, thus, within the stability
window of LLZO. The electrodes, prepared as either
conventional slurry mixture, thin films or spray-coating and
directly deposited on the surface of the electrolyte pellet,
show reversible electrochemical activity comparable to the
liquid counterpart except the possible absence of a solid
electrolyte interphase (SEI). For the first time, we discuss
the possibility to lithiate/delithiate reversibly
alloy-based nanoparticles in combination with the garnet
LLZO electrolyte and their interfacial stability. Such
investigation is supported by electrochemical
characterization coupled with surface and structural
characterization (XPS, SEM and XRD).},
month = {Jun},
date = {2017-06-18},
organization = {21st International Conference on Solid
State Ionics, Padua (Italy), 18 Jun
2017 - 23 Jun 2017},
subtyp = {Outreach},
cin = {IEK-1},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)24},
url = {https://juser.fz-juelich.de/record/834447},
}