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@ARTICLE{Rusu:836008,
author = {Rusu, M. I. and Pardanaud, C. and Ferro, Y. and Giacometti,
G. and Martin, C. and Addab, Y. and Roubin, P. and
Minissale, M. and Ferri, L. and Virot, F. and Barrachin, M.
and Lungu, C. P. and Porosnicu, C. and Dinca, P. and Lungu,
M. and Köppen, M. and Hansen, P. and Linsmeier, Ch.},
title = {{P}reparing the future post-mortem analysis of
beryllium-based {JET} and {ITER} samples by
multi-wavelengths {R}aman spectroscopy on implanted {B}e,
and co-deposited {B}e},
journal = {Nuclear fusion},
volume = {57},
number = {7},
issn = {1741-4326},
address = {Vienna},
publisher = {IAEA},
reportid = {FZJ-2017-05133},
pages = {076035},
year = {2017},
abstract = {This study demonstrates that Raman microscopy is a suitable
technique for future post mortem analyses of JET and ITER
plasma facing components. We focus here on laboratory
deposited and bombarded samples of beryllium and beryllium
carbides and start to build a reference spectral databases
for fusion relevant beryllium-based materials. We identified
the beryllium phonon density of states, its second harmonic
and E 2G and B 2G second harmonic and combination modes for
defective beryllium in the spectral range 300–700 and
700–1300 cm−1, lying close to Be–D modes of
beryllium hydrides. We also identified beryllium carbide
signature, Be2C, combining Raman microscopy and DFT
calculation. We have shown that, depending on the optical
constants of the material probed, in depth sensitivity at
the nanometer scale can be performed using different
wavelengths. This way, we demonstrate that multi-wavelength
Raman microscopy is sensitive to in-depth stress caused by
ion implantation (down to ≈30 nm under the surface
for Be) and Be/C concentration (down to 400 nm or more
under the surface for Be+C), which is a main contribution of
this work. The depth resolution reached can then be adapted
for studying the supersaturated surface layer found on
tokamak deposits.},
cin = {IEK-4},
ddc = {530},
cid = {I:(DE-Juel1)IEK-4-20101013},
pnm = {113 - Methods and Concepts for Material Development
(POF3-113)},
pid = {G:(DE-HGF)POF3-113},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000403048600001},
doi = {10.1088/1741-4326/aa70bb},
url = {https://juser.fz-juelich.de/record/836008},
}