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@ARTICLE{vonAspern:837181,
author = {von Aspern, Natascha and Röser, Stephan and Rezaei Rad,
Babak and Murmann, Patrick and Streipert, Benjamin and
Mönnighoff, Xaver and Tillmann, Selina Denise and Shevchuk,
Michael and Stubbmann-Kazakova, Olesya and Röschenthaler,
Gerd-Volker and Nowak, Sascha and Winter, Martin and
Cekic-Laskovic, Isidora},
title = {{P}hosphorus additives for improving high voltage stability
and safety of lithium ion batteries},
journal = {Journal of fluorine chemistry},
volume = {198},
issn = {0022-1139},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2017-06160},
pages = {24 - 33},
year = {2017},
abstract = {Three phosphorus containing molecules,
tris(2,2,3,3,3-pentafluoropropyl) phosphate (5F-TPrP),
tris(1,1,1,3,3,3-hexafluoropropan-2-yl) phosphate (HFiP) and
tris(1,1,1,3,3,3-hexafluoropropan-2-yl) phosphite (THFPP),
were investigated as high voltage and flame retardant
electrolyte additives for lithium ion batteries. The effect
of the oxidation state of the phosphorus atom as well as the
influence of branched vs. linear fluorinated propyl groups
were investigated regarding cycling performance and
flammability of the resulting electrolyte. In the case of a
high voltage battery application, all three investigated
molecules showed an improvement regarding the cycling
performance in NCM111/Li half-cells. Post mortem analysis of
the NCM111 electrodes via SEM and XPS indicates that the
different groups of two phosphates (5F-TPrP vs. HFiP) have
an impact on the thickness, morphology and composition of
the cathode electrolyte interphase (CEI). If the electrolyte
formulation contains the linear side group (5F-TPrP), the
thickness of the CEI increases, whereas for the branched
group (HFiP) it decreases compared to the CEI formed in 1 M
LiPF6 EC:DEC (1:1) used as reference electrolyte.
Furthermore, addition of at least 20 $wt.\%$ of 5F-TPrP to
the reference electrolyte formulation resulted in a
non-flammable electrolyte formulation.},
cin = {IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000405057800004},
doi = {10.1016/j.jfluchem.2017.02.005},
url = {https://juser.fz-juelich.de/record/837181},
}